(2R,6R,11R)-3,6,11-Trimethyl-9-nitro-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocine; compound with picric acid

Base Information

• Chemical Name: (2R,6R,11R)-3,6,11-Trimethyl-9-nitro-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocine; compound with picric acid
• CAS No.: 125424-08-0
• Molecular Formula: C₆H₃N₃O₇*C₁₅H₂₀N₂O₂
• Molecular Weight: 489.442
• Mol file: 125424-08-0.mol

Synonyms:

Chemical Property of (2R,6R,11R)-3,6,11-Trimethyl-9-nitro-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocine; compound with picric acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2R,6R,11R)-3,6,11-Trimethyl-9-nitro-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocine; compound with picric acid

There total 1 articles about (2R,6R,11R)-3,6,11-Trimethyl-9-nitro-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocine; compound with picric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-Trinitrophenol (88-89-1) + (2R,6R,11R)-3,6,11-Trimethyl-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocine (42529-29-3,53424-43-4,64023-76-3,64023-83-2,100937-89-1,144539-62-8) → (2R,6R,11R)-3,6,11-Trimethyl-8-nitro-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocine; compound with picric acid + (2R,6R,11R)-3,6,11-Trimethyl-9-nitro-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocine; compound with picric acid (125424-08-0)

Guidance literature:

With nitric acid; acetic acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) RT, overnight; 2.) acetone;

DOI:10.1248/cpb.37.2222

upstream raw materials:

2,4,6-Trinitrophenol

(2R,6R,11R)-3,6,11-Trimethyl-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocine