n-butyltris(triphenylethenyl)tin(IV)

Base Information

Chemical Name:n-butyltris(triphenylethenyl)tin(IV)
CAS No.:86297-62-3
Molecular Formula:C₆₄H₅₄Sn
Molecular Weight:941.843
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Chemical Property of n-butyltris(triphenylethenyl)tin(IV)

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Technology Process of n-butyltris(triphenylethenyl)tin(IV)

There total 1 articles about n-butyltris(triphenylethenyl)tin(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.7%

: 109-72-8,29786-93-4
n-butyllithium

: 1607-57-4
Triphenylvinyl bromide

: tin(ll) chloride

: 86297-62-3
n-butyltris(triphenylethenyl)tin(IV)

Guidance literature:: In tetrahydrofuran; diethyl ether; under argon to cooled in ethanol-dry-ice bromotriphenylethene in ether added dropwise n-butyl-lithium, suspn. stirred for 45 min at low temp. and 3 h at room temp., suspn. cooled, soln. SnCl2 in thf added dropwise and stirred for 1 h at low temp.; suspn. allowed to warm to room temp. over 2 h, volatiles removed under vac., toluene added to residue, stirred for 30 mn, mixt. filtered, toluene removed under vac., hexane added, suspn. filtered, solid recrystd. from hexane-toluene; elem. anal.;
DOI:10.1039/DT9830000665