Rhodanine, 5-(p-chlorobenzylidene)-3-(p-chlorobenzylideneamino)-

Base Information

• Chemical Name: Rhodanine, 5-(p-chlorobenzylidene)-3-(p-chlorobenzylideneamino)-
• CAS No.: 17521-25-4
• Molecular Formula: C₁₇H₁₀Cl₂N₂OS₂
• Molecular Weight: 393.317
• NSC Number: 231544
• DSSTox Substance ID: DTXSID20430623

Synonyms:NSC231544;17521-25-4;DTXSID20430623;AKOS027468338;NSC-231544;Rhodanine, 5-(p-chlorobenzylidene)-3-(p-chlorobenzylideneamino)-

Chemical Property of Rhodanine, 5-(p-chlorobenzylidene)-3-(p-chlorobenzylideneamino)-

Chemical Property:

• Vapor Pressure: 2.13E-11mmHg at 25°C
• Boiling Point: 532°C at 760 mmHg
• Flash Point: 275.5°C
• Density: 1.42g/cm³
• XLogP3: 5.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 391.9611607
• Heavy Atom Count: 24
• Complexity: 551

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C=C2C(=O)N(C(=S)S2)N=CC3=CC=C(C=C3)Cl)Cl
• Isomeric SMILES: C1=CC(=CC=C1/C=C/2\C(=O)N(C(=S)S2)/N=C/C3=CC=C(C=C3)Cl)Cl

Technology Process of Rhodanine, 5-(p-chlorobenzylidene)-3-(p-chlorobenzylideneamino)-

There total 3 articles about Rhodanine, 5-(p-chlorobenzylidene)-3-(p-chlorobenzylideneamino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chlorobenzaldehyde (104-88-1) → 5-(4-chloro-benzylidene)-3-(4-chloro-benzylideneamino)-2-thioxo-thiazolidin-4-one (17521-25-4)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol

2: NH₄OH

With ammonium hydroxide; In ethanol;

DOI:10.1007/BF00510013

Reference yield:

3-(4-chlorobenzylideneamino)-2-thioxothiazolidin-4-one (17492-66-9) + 4-chlorobenzaldehyde (104-88-1) → 5-(4-chloro-benzylidene)-3-(4-chloro-benzylideneamino)-2-thioxo-thiazolidin-4-one (17521-25-4)

Guidance literature:

With ammonium hydroxide;

DOI:10.1007/BF00510013

Reference yield:

→ 5-(4-chloro-benzylidene)-3-(4-chloro-benzylideneamino)-2-thioxo-thiazolidin-4-one (17521-25-4)

Guidance literature:

3-Amino-rhodanin, entsprech. substit. Aldehyd, sd. Essigsaeure;

DOI:10.1007/BF00481590

upstream raw materials:

3-(4-chlorobenzylideneamino)-2-thioxothiazolidin-4-one

4-chlorobenzaldehyde

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