Butyl 3-hydroxy-2-methylidenebutanoate

Base Information

Chemical Name:Butyl 3-hydroxy-2-methylidenebutanoate
CAS No.:22141-40-8
Molecular Formula:C₉H₁₆O₃
Molecular Weight:172.224
Hs Code.:2918199090
DSSTox Substance ID:DTXSID90340861
Nikkaji Number:J283.648C
Wikidata:Q82110720
Metabolomics Workbench ID:48901
Mol file:22141-40-8.mol

Synonyms:butyl 3-hydroxy-2-methylidenebutanoate;Butyl 3-hydroxy-2-methylene-butanoate;22141-40-8;Isobutylester of 3-Hydroxy-2-methylidenebutryric acid;SCHEMBL5248798;DTXSID90340861;CHEBI:171941;Butyl 2-(1-hydroxyethyl)acrylate #;3-Hydroxy-2-methylenebutyric acid butyl ester;3-Hydroxy-2-methylene-butyric acid butyl ester;3-Hydroxy-2-methylenebutanoic acid butyl ester;Butanoic acid, 3-hydroxy-2-methylene-, butyl ester;Butyric acid, 3-hydroxy-2-methylene-, butyl ester

Suppliers and Price of Butyl 3-hydroxy-2-methylidenebutanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Butyl 3-hydroxy-2-methylidenebutanoate

Chemical Property:

PSA：46.53000
LogP:1.26670
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:172.109944368
Heavy Atom Count:12
Complexity:163

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCOC(=O)C(=C)C(C)O

Technology Process of Butyl 3-hydroxy-2-methylidenebutanoate

There total 3 articles about Butyl 3-hydroxy-2-methylidenebutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37981-18-3
5-norbornene-2-butyl ester

: 22141-40-8
3-hydroxy-2-methylidenbuttersaeurebutylester

Guidance literature:: Multi-step reaction with 2 steps

1: LDA / hexane; diethyl ether; 1,2-dimethoxy-ethane / -70 °C

2: Retro Dien synthesis with heating

With lithium diisopropyl amide; In 1,2-dimethoxyethane; diethyl ether; hexane;
DOI:10.1002/hlca.19810640739