3-(Naphthalen-1-ylamino)propan-1-ol

Base Information

• Chemical Name: 3-(Naphthalen-1-ylamino)propan-1-ol
• CAS No.: 6628-35-9
• Molecular Formula: C13H15 N O
• Molecular Weight: 201.268
• NSC Number: 60580
• DSSTox Substance ID: DTXSID70289380
• Nikkaji Number: J2.388.142J
• Wikidata: Q82026658

Synonyms:6628-35-9;NSC 60580;3-(naphthalen-1-ylamino)propan-1-ol;NSC60580;SCHEMBL11111574;DTXSID70289380;3-(1-Naphthylamino)-1-propanol;NSC-60580;AKOS009030630

Chemical Property of 3-(Naphthalen-1-ylamino)propan-1-ol

Chemical Property:

• Vapor Pressure: 2.2E-07mmHg at 25°C
• Boiling Point: 407.9°Cat760mmHg
• Flash Point: 184°C
• Density: 1.159g/cm³
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 201.115364102
• Heavy Atom Count: 15
• Complexity: 183

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC=C2NCCCO

Technology Process of 3-(Naphthalen-1-ylamino)propan-1-ol

There total 5 articles about 3-(Naphthalen-1-ylamino)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

naphthalene (91-20-3,71998-51-1,72931-45-4) + 2-Phenyl-5,6-dihydro-4H-[1,3]oxazine (3420-41-5) → 3-(naphthalen-1-ylamino)propan-1-ol (6628-35-9)

Guidance literature:

naphthalene; 2-Phenyl-5,6-dihydro-4H-[1,3]oxazine; With lithium perchlorate; In acetonitrile; at 0 ℃; Inert atmosphere; Electrochemical reaction;

With ethylenediamine; In acetonitrile; at 70 ℃; for 3h; chemoselective reaction; Inert atmosphere;

DOI:10.1021/jacs.5b06526

Reference yield: 70.0%

1-amino-naphthalene (134-32-7) + 1-bromo-3-propanol (627-18-9) → 3-(naphthalen-1-ylamino)propan-1-ol (6628-35-9)

Guidance literature:

In ethanol; for 15h; Heating;

DOI:10.1016/j.tet.2006.12.005

Reference yield: 68.0%

1-amino-naphthalene (134-32-7) + trimethyleneglycol (504-63-2) → 7,8-benzoquinoline (230-27-3) + 3-(naphthalen-1-ylamino)propan-1-ol (6628-35-9)

Guidance literature:

With tetrafluoroboric acid diethyl ether; {[(PCy₃)(CO)RuH]₄(μ-O)(μ-OH)₂}; cyclopentene; In 1,4-dioxane; at 130 ℃; for 14h; regioselective reaction; Sealed tube; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.organomet.6b00273

upstream raw materials:

[1]naphthyl-carbamic acid-(3-chloro-propyl ester)

1-amino-naphthalene

1-bromo-3-propanol

naphthalene

Downstream raw materials:

7,8-benzoquinoline

1-amino-naphthalene

N¹,N³-di(naphthalen-1-yl)propane-1,3-diamine

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