3-Nitro-2-bornanone

Base Information

• Chemical Name: 3-Nitro-2-bornanone
• CAS No.: 2243-88-1
• Molecular Formula: C10H15NO3
• Molecular Weight: 197.234
• Hs Code.: 2914700090
• Mol file: 2243-88-1.mol

Synonyms:3-Nitro-campher;3-nitro-bornan-2-one;3-Nitro-bornan-2-on;2-Bornanone,3-nitro-,d;3-nitrocamphor;

Chemical Property of 3-Nitro-2-bornanone

Chemical Property:

• PSA: 62.89000
• LogP: 2.18010

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Nitro-2-bornanone

There total 7 articles about 3-Nitro-2-bornanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

tetranitromethane (509-14-8) + camphor trimethylsilyl enol ether (56613-17-3) → trinitromethane (517-25-9,57073-37-7) + 3-nitrocamphor (2243-88-1)

Guidance literature:

In dichloromethane; at -30 ℃; for 0.3h;

DOI:10.1021/jo9515687

Reference yield: 54.0%

camphor trimethylsilyl enol ether (56613-17-3) → 3-nitrocamphor (2243-88-1)

Guidance literature:

With tetranitromethane; In pentane; at -30 ℃; for 3h;

DOI:10.1016/S0040-4039(00)91947-6

Reference yield:

→ 3-nitrocamphor (2243-88-1)

Guidance literature:

With diethyl ether; sulfuric acid; zinc; α-nitro-d-camphor;

upstream raw materials:

(1R,E)-(+)-camphorquinone 3-oxime

camphor trimethylsilyl enol ether

tetranitromethane

Downstream raw materials:

camphoric anhydride

2,2-dimethyl-cyclopentane-1,1,3-tricarboxylic acid

ammonia

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