Carbonic acid 2-(4-cyano-2-nitro-phenyl)-ethyl ester (2R,3S,5R)-3-hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

Base Information

• Chemical Name: Carbonic acid 2-(4-cyano-2-nitro-phenyl)-ethyl ester (2R,3S,5R)-3-hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester
• CAS No.: 215600-48-9
• Molecular Formula: C₂₀H₂₀N₄O₉
• Molecular Weight: 460.4

Synonyms:

Chemical Property of Carbonic acid 2-(4-cyano-2-nitro-phenyl)-ethyl ester (2R,3S,5R)-3-hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

Chemical Property:

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Technology Process of Carbonic acid 2-(4-cyano-2-nitro-phenyl)-ethyl ester (2R,3S,5R)-3-hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

There total 3 articles about Carbonic acid 2-(4-cyano-2-nitro-phenyl)-ethyl ester (2R,3S,5R)-3-hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-cyano-2-nitrotoluene (939-79-7) → Carbonic acid 2-(4-cyano-2-nitro-phenyl)-ethyl ester (2R,3S,5R)-3-hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester (215600-48-9)

Guidance literature:

DOI:10.1080/07328319808004738

Reference yield:

4-(2-hydroxyethyl)-3-nitrobenzonitrile (69395-14-8) → Carbonic acid 2-(4-cyano-2-nitro-phenyl)-ethyl ester (2R,3S,5R)-3-hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester (215600-48-9)

Guidance literature:

DOI:10.1080/07328319808004738

Reference yield:

C10H7ClN2O4 + thymidine (50-89-5,28854-96-8,3545-96-8,50-88-4) → Carbonic acid 2-(4-cyano-2-nitro-phenyl)-ethyl ester (2R,3S,5R)-2-hydroxymethyl-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester + Carbonic acid 2-(4-cyano-2-nitro-phenyl)-ethyl ester (2R,3S,5R)-3-hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester (215600-48-9) + Carbonic acid (2R,3S,5R)-2-[2-(4-cyano-2-nitro-phenyl)-ethoxycarbonyloxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-(4-cyano-2-nitro-phenyl)-ethyl ester

Guidance literature:

Yield given;

DOI:10.1080/07328319808004738

upstream raw materials:

thymidine

4-cyano-2-nitrotoluene

4-(2-hydroxyethyl)-3-nitrobenzonitrile

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