Lithium 2-(dimethylamino)benzen-1-ide

Base Information

Chemical Name:Lithium 2-(dimethylamino)benzen-1-ide
CAS No.:22608-37-3
Molecular Formula:C8H10LiN
Molecular Weight:127.115
Hs Code.:
DSSTox Substance ID:DTXSID90504603
Mol file:22608-37-3.mol

Synonyms:22608-37-3;Lithium 2-(dimethylamino)benzen-1-ide;2-lithiodi-methylaminobenzene;SCHEMBL1136914;DTXSID90504603

Suppliers and Price of Lithium 2-(dimethylamino)benzen-1-ide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Lithium 2-(dimethylamino)benzen-1-ide

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:127.09732776
Heavy Atom Count:10
Complexity:178

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:[Li+].CN(C)C1=CC=CC=[C-]1

Technology Process of Lithium 2-(dimethylamino)benzen-1-ide

There total 4 articles about Lithium 2-(dimethylamino)benzen-1-ide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 698-00-0
2-bromo-N,N-dimethylaniline

: 22608-37-3
ortho-lithio-N,N-dimethylaniline

Guidance literature:: With n-butyllithium; In hexane; for 3.25h; Inert atmosphere; Cooling with ice;
DOI:10.1039/c2dt30926b

Reference yield: 73.0%

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 22608-37-3
ortho-lithio-N,N-dimethylaniline

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; at 70 - 75 ℃; for 36h; Solvent; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1039/c6dt04649e