tetra-O-acetyl-6-iodo-aldehydo-6-deoxy-D-glucose-dibenzyldithioacetal

Base Information

• Chemical Name: tetra-O-acetyl-6-iodo-aldehydo-6-deoxy-D-glucose-dibenzyldithioacetal
• CAS No.: 124103-92-0
• Molecular Formula: C₂₈H₃₃IO₈S₂
• Molecular Weight: 688.602
• Mol file: 124103-92-0.mol

Synonyms:

Chemical Property of tetra-O-acetyl-6-iodo-aldehydo-6-deoxy-D-glucose-dibenzyldithioacetal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetra-O-acetyl-6-iodo-aldehydo-6-deoxy-D-glucose-dibenzyldithioacetal

There total 3 articles about tetra-O-acetyl-6-iodo-aldehydo-6-deoxy-D-glucose-dibenzyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylmethanethiol (100-53-8) → tetra-O-acetyl-6-iodo-aldehydo-6-deoxy-D-glucose-dibenzyldithioacetal (124103-92-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium methylate; methanol; concentrated aqueous HCl / Reaktion ueber 2 Stufen

2: pyridine

With pyridine; hydrogenchloride; methanol; sodium methylate;

Reference yield:

6-deoxy-6-iodotetra-O-acetyl-β-D-glucopyranose (7468-48-6) → tetra-O-acetyl-6-iodo-aldehydo-6-deoxy-D-glucose-dibenzyldithioacetal (124103-92-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium methylate; methanol; concentrated aqueous HCl / Reaktion ueber 2 Stufen

2: pyridine

With pyridine; hydrogenchloride; methanol; sodium methylate;

Reference yield:

6-iodo-6-deoxy-D-glucose-dibenzyldithioacetal (111325-55-4) + acetic anhydride (108-24-7) → tetra-O-acetyl-6-iodo-aldehydo-6-deoxy-D-glucose-dibenzyldithioacetal (124103-92-0)

Guidance literature:

With pyridine;

upstream raw materials:

6-iodo-6-deoxy-D-glucose-dibenzyldithioacetal

acetic anhydride

phenylmethanethiol

6-deoxy-6-iodotetra-O-acetyl-β-D-glucopyranose