Benzaldehyde, 4-hydroxy-, sodium salt

Base Information

• Chemical Name: Benzaldehyde, 4-hydroxy-, sodium salt
• CAS No.: 22666-84-8
• Molecular Formula: C7H6O2.Na
• Molecular Weight: 144.105
• Mol file: 22666-84-8.mol

Synonyms:

Chemical Property of Benzaldehyde, 4-hydroxy-, sodium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzaldehyde, 4-hydroxy-, sodium salt

There total 4 articles about Benzaldehyde, 4-hydroxy-, sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

phenyl 4-formylphenyl carbonate (1268380-08-0) → sodium salicylat (81256-74-8) + 4-hydroxybenzaldehyde sodium salt (22666-84-8)

Guidance literature:

With water; sodium hydroxide; In dimethyl sulfoxide; at 25 ℃; Kinetics;

DOI:10.5012/bkcs.2010.31.7.2015

Reference yield:

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 4-hydroxybenzaldehyde sodium salt (22666-84-8)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.666667h;

Reference yield:

sodium p-oxybenzaldehyde hydrate → 4-hydroxybenzaldehyde sodium salt (22666-84-8)

Guidance literature:

In neat (no solvent, solid phase); at 60 ℃; Sealed tube;

DOI:10.1039/c4dt02941k

upstream raw materials:

4-hydroxy-benzaldehyde

phenyl 4-formylphenyl carbonate

Downstream raw materials:

Thiocarbonic acid O,O-bis-(4-formyl-phenyl) ester

p-formylphenyl p-iodophenylcarbamoylmethyl ether

p-formylphenyl p-chlorophenylcarbamoylmethyl ether

p-formylphenyl p-bromophenylcarbamoylmethyl ether

Refernces

• 1、 -. "Isoniazide-heptamethine indocyanine coupling compound as well as preparation method and application thereof". Paragraph 0062; 0070-0072. . Retrieved 2020/05/11.
• 2、 Kim, Song-I,Hwang, So-Jeong,Jung, Eun-Mi,Um, Ik-Hwan. "Kinetics and mechanism of alkaline hydrolysis of Y-substituted phenyl phenyl carbonates". experimental part. p. 2015 - 2018. Retrieved 2010/12/19.