1,3-Propanediol, 2-amino-1-(4-nitrophenyl)-, monohydrochloride

Base Information

Chemical Name:1,3-Propanediol, 2-amino-1-(4-nitrophenyl)-, monohydrochloride
CAS No.:2271-58-1
Molecular Formula:C₉H₁₂N₂O₄*ClH
Molecular Weight:248.666
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Propanediol, 2-amino-1-(4-nitrophenyl)-, monohydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-Propanediol, 2-amino-1-(4-nitrophenyl)-, monohydrochloride

There total 5 articles about 1,3-Propanediol, 2-amino-1-(4-nitrophenyl)-, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 2271-58-1,3532-63-6,6460-74-8,19534-26-0,21791-98-0,35530-10-0,99091-18-6
(1RS,2RS)-2-amino-1-(4-nitro-phenyl)-propane-1,3-diol; hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / Hydrogen peroxide, hydrobromic acid / 3 h / 90 - 95 °C

2: 84 percent / Potasium hydrogen sulfate, hydroquinone / H₂O / 150 - 185 °C

3: 90 percent / Sulfuric acid / H₂O / 6.5 h / 50 °C

4: 75 percent / Anhydrous ammonia / methanol / 14 h / 150 °C / 45003.6 - 52504.2 Torr

5: Fuming nitric acid, acetic anhydride, 30percent hydrochloric acid / 1) 0 deg C, 1 h, 2) 20 deg C, 2 h, 3) 166 - 170 deg C, 30percent hydrochloric acid

With hydrogenchloride; potassium hydrogensulfate; sulfuric acid; ammonia; hydrogen bromide; dihydrogen peroxide; nitric acid; acetic anhydride; hydroquinone; In methanol; water;

Reference yield:

: 77940-37-5
5-bromo-4-phenyl-[1,3]dioxane

: 2271-58-1,3532-63-6,6460-74-8,19534-26-0,21791-98-0,35530-10-0,99091-18-6
(1RS,2RS)-2-amino-1-(4-nitro-phenyl)-propane-1,3-diol; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Anhydrous ammonia / methanol / 14 h / 150 °C / 45003.6 - 52504.2 Torr

2: Fuming nitric acid, acetic anhydride, 30percent hydrochloric acid / 1) 0 deg C, 1 h, 2) 20 deg C, 2 h, 3) 166 - 170 deg C, 30percent hydrochloric acid

With hydrogenchloride; ammonia; nitric acid; acetic anhydride; In methanol;

Reference yield:

: 103-64-0,1340-14-3
bromostyrene

: 2271-58-1,3532-63-6,6460-74-8,19534-26-0,21791-98-0,35530-10-0,99091-18-6
(1RS,2RS)-2-amino-1-(4-nitro-phenyl)-propane-1,3-diol; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / Sulfuric acid / H₂O / 6.5 h / 50 °C

2: 75 percent / Anhydrous ammonia / methanol / 14 h / 150 °C / 45003.6 - 52504.2 Torr

3: Fuming nitric acid, acetic anhydride, 30percent hydrochloric acid / 1) 0 deg C, 1 h, 2) 20 deg C, 2 h, 3) 166 - 170 deg C, 30percent hydrochloric acid

With hydrogenchloride; sulfuric acid; ammonia; nitric acid; acetic anhydride; In methanol; water;