quinuclidin-4-aMine

Base Information

• Chemical Name: quinuclidin-4-aMine
• CAS No.: 22766-61-6
• Molecular Formula: C₇H₁₄N₂
• Molecular Weight: 126.202
• Mol file: 22766-61-6.mol

Synonyms:4-Amino-chinuclidin;p-Carboxamido-phenoxiessigsaeure;4-aminochalcone;4-Carbamoylphenoxy-essigsaeure;4-Amino-chalkon;

Chemical Property of quinuclidin-4-aMine

Chemical Property:

• Vapor Pressure: 1.48mmHg at 25°C
• Boiling Point: 170.2oC at 760 mmHg
• PKA: 10.13±0.12(Predicted)
• Flash Point: 53oC
• PSA: 29.26000
• Density: 1.07g/cm3
• LogP: 0.82160

Purity/Quality:

97% ^*data from raw suppliers

1-azabicyclo[2.2.2]octan-4-amine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of quinuclidin-4-aMine

There total 1 articles about quinuclidin-4-aMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 4-aminoquinuclidine (22766-61-6)

Guidance literature:

4-Ethoxycarbonylamino-chinuclidin, sd. konz. HCl (10h; Ausb. etwa 95percent; Hydrolyse);

DOI:10.1007/BF00943918

Reference yield:

4-aminoquinuclidine (22766-61-6) → 4-amino-N-(1-azabicyclo[2.2.2]oct-4-yl)-5-chloro-2-methoxybenzamide (106792-80-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / toluene / 4 h / Ambient temperature

2: 2.5 N NaOH / ethanol / 2 h / Heating

With sodium hydroxide; triethylamine; In ethanol; toluene;

DOI:10.1021/jm00058a004

Reference yield:

4-acetylamino-5-chloro-2-methoxy-benzoyl chloride (4516-32-9) + 4-aminoquinuclidine (22766-61-6) → 4-Acetylamino-N-(1-aza-bicyclo[2.2.2]oct-4-yl)-5-chloro-2-methoxy-benzamide

Guidance literature:

With triethylamine; In toluene; for 4h; Ambient temperature;

DOI:10.1021/jm00058a004

Downstream raw materials:

4-amino-N-(1-azabicyclo[2.2.2]oct-4-yl)-5-chloro-2-methoxybenzamide

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