6-(5-azido-4-benzyloxy-6-methoxy-2-sulfooxymethyl-tetrahydro-pyran-3-yloxy)-3-[3-azido-4-benzyloxy-5-(naphthalen-2-ylmethoxy)-6-sulfooxymethyl-tetrahydro-pyran-2-yloxy]-4-benzyloxy-5-sulfooxy-tetrahydro-pyran-2-carboxylic acid

Base Information

• Chemical Name: 6-(5-azido-4-benzyloxy-6-methoxy-2-sulfooxymethyl-tetrahydro-pyran-3-yloxy)-3-[3-azido-4-benzyloxy-5-(naphthalen-2-ylmethoxy)-6-sulfooxymethyl-tetrahydro-pyran-2-yloxy]-4-benzyloxy-5-sulfooxy-tetrahydro-pyran-2-carboxylic acid
• CAS No.: 657395-23-8
• Molecular Formula: C₅₁H₅₆N₆O₂₄S₃
• Molecular Weight: 1233.23

Synonyms:

Chemical Property of 6-(5-azido-4-benzyloxy-6-methoxy-2-sulfooxymethyl-tetrahydro-pyran-3-yloxy)-3-[3-azido-4-benzyloxy-5-(naphthalen-2-ylmethoxy)-6-sulfooxymethyl-tetrahydro-pyran-2-yloxy]-4-benzyloxy-5-sulfooxy-tetrahydro-pyran-2-carboxylic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of 6-(5-azido-4-benzyloxy-6-methoxy-2-sulfooxymethyl-tetrahydro-pyran-3-yloxy)-3-[3-azido-4-benzyloxy-5-(naphthalen-2-ylmethoxy)-6-sulfooxymethyl-tetrahydro-pyran-2-yloxy]-4-benzyloxy-5-sulfooxy-tetrahydro-pyran-2-carboxylic acid

There total 3 articles about 6-(5-azido-4-benzyloxy-6-methoxy-2-sulfooxymethyl-tetrahydro-pyran-3-yloxy)-3-[3-azido-4-benzyloxy-5-(naphthalen-2-ylmethoxy)-6-sulfooxymethyl-tetrahydro-pyran-2-yloxy]-4-benzyloxy-5-sulfooxy-tetrahydro-pyran-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl [2-azido-3-O-benzyl-2-deoxy-4-O-(2-naphthylmethyl)-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosyluronicacid)-(1->4)-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranoside (657395-22-7) → 6-(5-azido-4-benzyloxy-6-methoxy-2-sulfooxymethyl-tetrahydro-pyran-3-yloxy)-3-[3-azido-4-benzyloxy-5-(naphthalen-2-ylmethoxy)-6-sulfooxymethyl-tetrahydro-pyran-2-yloxy]-4-benzyloxy-5-sulfooxy-tetrahydro-pyran-2-carboxylic acid (657395-23-8)

Guidance literature:

With sulfur trioxide; triethylamine;

DOI:10.1002/jccs.200400175

Reference yield:

methyl [2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-4-O-(2-naphthylmethyl)-α-D-glucopyranosyl]-(1->4)-(2-O-benzoyl-3-O-benzyl-α-L-idopyranosyl)-(1->4)-2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranoside (657395-21-6) → 6-(5-azido-4-benzyloxy-6-methoxy-2-sulfooxymethyl-tetrahydro-pyran-3-yloxy)-3-[3-azido-4-benzyloxy-5-(naphthalen-2-ylmethoxy)-6-sulfooxymethyl-tetrahydro-pyran-2-yloxy]-4-benzyloxy-5-sulfooxy-tetrahydro-pyran-2-carboxylic acid (657395-23-8)

Guidance literature:

Multi-step reaction with 3 steps

1: TEMPO; aq. NaOCl

2: NaOMe

3: SO₃; Et₃N

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sulfur trioxide; sodium methylate; triethylamine;

DOI:10.1002/jccs.200400175

Reference yield:

methyl [2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-4-O-(2-naphthylmethyl)-α-D-glucopyranosyl]-(1->4)-(2-O-benzoyl-3-O-benzyl-α-L-idopyranosyluronicacid)-(1->4)-2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranoside (657395-12-5) → 6-(5-azido-4-benzyloxy-6-methoxy-2-sulfooxymethyl-tetrahydro-pyran-3-yloxy)-3-[3-azido-4-benzyloxy-5-(naphthalen-2-ylmethoxy)-6-sulfooxymethyl-tetrahydro-pyran-2-yloxy]-4-benzyloxy-5-sulfooxy-tetrahydro-pyran-2-carboxylic acid (657395-23-8)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOMe

2: SO₃; Et₃N

With sulfur trioxide; sodium methylate; triethylamine;

DOI:10.1002/jccs.200400175

upstream raw materials:

methyl [2-azido-3-O-benzyl-2-deoxy-4-O-(2-naphthylmethyl)-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosyluronicacid)-(1->4)-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranoside

methyl [2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-4-O-(2-naphthylmethyl)-α-D-glucopyranosyl]-(1->4)-(2-O-benzoyl-3-O-benzyl-α-L-idopyranosyl)-(1->4)-2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranoside

methyl [2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-4-O-(2-naphthylmethyl)-α-D-glucopyranosyl]-(1->4)-(2-O-benzoyl-3-O-benzyl-α-L-idopyranosyluronicacid)-(1->4)-2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranoside

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