Phenylalanine, monosodium salt

Base Information

• Chemical Name: Phenylalanine, monosodium salt
• CAS No.: 23338-68-3
• Molecular Formula: C9H11NO2.Na
• Molecular Weight: 187.174
• Mol file: 23338-68-3.mol

Synonyms:

Chemical Property of Phenylalanine, monosodium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phenylalanine, monosodium salt

There total 2 articles about Phenylalanine, monosodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylalanine enamine of ethylacetoacetate sodium salt (75428-57-8) → ethyl acetoacetate (141-97-9) + β-phenylalanine sodium salt (23338-68-3)

Guidance literature:

In water; at 37 ℃; for 4h; Equilibrium constant; pH:7.0-9.75; effect of pH;

DOI:10.1248/cpb.32.4545

Reference yield:

phenylalanine ethyl ester (1795-96-6) → β-phenylalanine sodium salt (23338-68-3)

Guidance literature:

With water; sodium hydroxide; for 0.00416667h; pH=12.2;

Reference yield: 95.0%

bis(trichloromethyl) carbonate (32315-10-9) + β-phenylalanine sodium salt (23338-68-3) → β-phenylalanine-NCA (90924-47-3)

Guidance literature:

With 4-methyl-morpholine; In water; acetonitrile; at 20 ℃; for 2.77778E-05h; Reagent/catalyst; Time; Flow reactor;

DOI:10.1002/asia.201901429

upstream raw materials:

phenylalanine enamine of ethylacetoacetate sodium salt

phenylalanine ethyl ester

Downstream raw materials:

8-benzyl-1,4,6-trioxa-9-aza-5λ⁵-phospha-spiro[4.4]nonan-7-one

DL-phenylalanine ethylacetoacetate enamine

phenylalanine enamine of ethylacetoacetate sodium salt

D-(R)-phenylalanine