(3-Chlorophenyl)phosphane

Base Information

Chemical Name:(3-Chlorophenyl)phosphane
CAS No.:23415-73-8
Molecular Formula:C6H6ClP
Molecular Weight:144.54
Hs Code.:
DSSTox Substance ID:DTXSID90591598
Nikkaji Number:J2.131.711J
Wikidata:Q82485394
Mol file:23415-73-8.mol

Synonyms:(3-Chlorophenyl)phosphane;Phosphine, (3-chlorophenyl)-;23415-73-8;SCHEMBL8461049;DTXSID90591598

Suppliers and Price of (3-Chlorophenyl)phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of (3-Chlorophenyl)phosphane

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:143.9895649
Heavy Atom Count:8
Complexity:74.9

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)Cl)P

Technology Process of (3-Chlorophenyl)phosphane

There total 2 articles about (3-Chlorophenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.5%

: 449764-31-2
tetramethyl (5-chloro-1,3-phenylene)bis[phosphonate]

: 23415-73-8
(3-chlorophenyl)phosphine

: (5-chloro-1,3-phenylene)bis[phosphine]

Guidance literature:: With lithium aluminium tetrahydride; chloro-trimethyl-silane; In tetrahydrofuran; at 20 ℃; for 36h;
DOI:10.1002/1522-2675(200204)85:4<1140::AID-HLCA1140>3.0.CO;2-X

Reference yield:

: 108-70-3,63697-19-8
1,3,5-trichlorobenzene

: 23415-73-8
(3-chlorophenyl)phosphine

Guidance literature:: Multi-step reaction with 2 steps

1: 35.4 percent / 504000 h / 50 °C / Irradiation

2: LiAlH₄; chlorotrimethylsilane / tetrahydrofuran / 36 h / 20 °C

With lithium aluminium tetrahydride; chloro-trimethyl-silane; In tetrahydrofuran; 1: photo-Arbuzov reaction;
DOI:10.1002/1522-2675(200204)85:4<1140::AID-HLCA1140>3.0.CO;2-X