(meso-cis-2,10-diphenyl-6-aza-kN-2,10-diphospha-k2P-bicyclo(9.4.0)pentadeca-11⁽¹⁾,12,14-triene)-(bicyclo(2.2.1)heptadiene)rhodium(I) hexafluorophosphate

Base Information

• Chemical Name: (meso-cis-2,10-diphenyl-6-aza-kN-2,10-diphospha-k2P-bicyclo(9.4.0)pentadeca-11⁽¹⁾,12,14-triene)-(bicyclo(2.2.1)heptadiene)rhodium(I) hexafluorophosphate
• CAS No.: 125837-02-7
• Molecular Formula: C₃₁H₃₅NP₂Rh*F₆P
• Molecular Weight: 731.443

Synonyms:

Chemical Property of (meso-cis-2,10-diphenyl-6-aza-kN-2,10-diphospha-k2P-bicyclo(9.4.0)pentadeca-11⁽¹⁾,12,14-triene)-(bicyclo(2.2.1)heptadiene)rhodium(I) hexafluorophosphate

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of (meso-cis-2,10-diphenyl-6-aza-kN-2,10-diphospha-k2P-bicyclo(9.4.0)pentadeca-11⁽¹⁾,12,14-triene)-(bicyclo(2.2.1)heptadiene)rhodium(I) hexafluorophosphate

There total 1 articles about (meso-cis-2,10-diphenyl-6-aza-kN-2,10-diphospha-k2P-bicyclo(9.4.0)pentadeca-11⁽¹⁾,12,14-triene)-(bicyclo(2.2.1)heptadiene)rhodium(I) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,4,5,6,7,8,9-octahydro-1,9-diphenyl-1H-5,1,9-benzazadiphosphacyclo undecine (125398-40-5) + (norbornadiene)2RhPF6 (38816-56-7) → (meso-cis-2,10-diphenyl-6-aza-kN-2,10-diphospha-k2P-bicyclo(9.4.0)pentadeca-11(1),12,14-triene)-(bicyclo(2.2.1)heptadiene)rhodium(I) hexafluorophosphate (125837-02-7)

Guidance literature:

In dichloromethane; addn. of a soln. of Rh-compound in CH2Cl2 under N2 to a soln. of ligand in CH2Cl2; addn. of a small portion of ethanol;

DOI:10.1016/0022-328X(89)85324-0

upstream raw materials:

2,3,4,5,6,7,8,9-octahydro-1,9-diphenyl-1H-5,1,9-benzazadiphosphacyclo undecine

(norbornadiene)2RhPF₆

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