3-(methylcarbamoyl)benzoic Acid

Base Information

Chemical Name:3-(methylcarbamoyl)benzoic Acid
CAS No.:23754-43-0
Molecular Formula:C9H9NO3
Molecular Weight:179.175
Hs Code.:
European Community (EC) Number:835-759-4
DSSTox Substance ID:DTXSID90452958
Wikidata:Q82273876
Mol file:23754-43-0.mol

Synonyms:3-(methylcarbamoyl)benzoic Acid;23754-43-0;Benzoic acid, 3-[(methylamino)carbonyl]-;N-methyl-isophthalamic acid;3-(methylcarbamoyl)benzoicAcid;SCHEMBL1200585;DTXSID90452958;ISDXXBVYCIDTIV-UHFFFAOYSA-N;AKOS008131971;EN300-90489;Z425331720

Suppliers and Price of 3-(methylcarbamoyl)benzoic Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-(methylcarbamoyl)benzoic Acid

Chemical Property:

XLogP3:0.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:179.058243149
Heavy Atom Count:13
Complexity:215

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNC(=O)C1=CC(=CC=C1)C(=O)O

Technology Process of 3-(methylcarbamoyl)benzoic Acid

There total 4 articles about 3-(methylcarbamoyl)benzoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 392743-67-8
isophthalamic acid methyl benzyl diester

: 23754-43-0
3-(methylcarbamoyl)benzoic acid

Guidance literature:: With hydrogen; 10percent Pd/C; In methanol; for 2h; under 2068.65 Torr;
DOI:10.1039/b105412k

Reference yield: 83.0%

: 23668-00-0
3-(N-methylaminocarbonyl)benzoic acid methyl ester

: 23754-43-0
3-(methylcarbamoyl)benzoic acid

Guidance literature:: With lithium hydroxide; In ethanol; at 20 ℃; for 1.5h;

Reference yield:

: 67852-96-4
3-(benzyloxycarbonyl)benzoyl chloride

: 23754-43-0
3-(methylcarbamoyl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 0.81 g / H₂O; CH₂Cl₂ / 1 h / 0 °C

2: 92 percent / H₂ / 10percent Pd/C / methanol / 2 h / 2068.65 Torr

With hydrogen; 10percent Pd/C; In methanol; dichloromethane; water;
DOI:10.1039/b105412k