N,N',N''-{Phosphanetriyltris[(2,1-phenylene)methylene]}tris(N-methylmethanamine)

Base Information

Chemical Name:N,N',N''-{Phosphanetriyltris[(2,1-phenylene)methylene]}tris(N-methylmethanamine)
CAS No.:23936-58-5
Molecular Formula:C27H36N3P
Molecular Weight:433.577
Hs Code.:
DSSTox Substance ID:DTXSID00578956
Nikkaji Number:J1.537.952I
Wikidata:Q82469305
Mol file:23936-58-5.mol

Synonyms:23936-58-5;DTXSID00578956;N,N',N''-{Phosphanetriyltris[(2,1-phenylene)methylene]}tris(N-methylmethanamine)

Suppliers and Price of N,N',N''-{Phosphanetriyltris[(2,1-phenylene)methylene]}tris(N-methylmethanamine)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,N',N''-{Phosphanetriyltris[(2,1-phenylene)methylene]}tris(N-methylmethanamine)

Chemical Property:

Boiling Point:501.8±50.0 °C(Predicted)
PSA：23.31000
LogP:3.62960
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:9
Exact Mass:433.26468516
Heavy Atom Count:31
Complexity:437

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)CC1=CC=CC=C1P(C2=CC=CC=C2CN(C)C)C3=CC=CC=C3CN(C)C

Technology Process of N,N',N''-{Phosphanetriyltris[(2,1-phenylene)methylene]}tris(N-methylmethanamine)

There total 1 articles about N,N',N''-{Phosphanetriyltris[(2,1-phenylene)methylene]}tris(N-methylmethanamine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 56174-66-4
2-(N,N-dimethylaminomethyl)phenyllithium

: 23936-58-5
Tris<2-(dimethylaminomethyl)phenyl>phosphan

Guidance literature:: With phosphorus tribromide; In diethyl ether; for 2h; Heating;

Reference yield: 95.0%

: 620591-69-7
silver(I) 3-hydroxy-2-methyl-γ-pyranoate

: 23936-58-5
Tris<2-(dimethylaminomethyl)phenyl>phosphan

: 680602-21-5
(P(C₆H₄CH₂N(CH₃)2)3)Ag(C₆H₅O₃)

Guidance literature:: In tetrahydrofuran; Ag-salt was added under N2 to a soln. the phosphine in THF in the dark at 25°C, stirred for 2 h; filtd. through a Celite pad, evapd. in vacuo, residue was washed with pentane; elem. anal.;
DOI:10.1016/S0020-1693(02)01500-1

Reference yield: 94.0%

: 620591-70-0
C₁₄H₆(O)2(OAg)2

: 23936-58-5
Tris<2-(dimethylaminomethyl)phenyl>phosphan

: 680602-24-8
((P(C₆H₄CH₂N(CH₃)2)3)Ag)2(C₁₄H₆O₄)

Guidance literature:: In tetrahydrofuran; Ag-salt was added under N2 to a soln. the phosphine in THF in the dark at 25°C, refluxed for 3 h; filtd. through a Celite pad, evapd. in vacuo, residue was washed with pentane; elem. anal.;
DOI:10.1016/S0020-1693(02)01500-1