2-(2-aminophenoxy)-N,N-dimethylacetamide

Base Information

Chemical Name:2-(2-aminophenoxy)-N,N-dimethylacetamide
CAS No.:24011-74-3
Molecular Formula:C10H14N2O2
Molecular Weight:194.233
Hs Code.:
Mol file:24011-74-3.mol

Synonyms:N,N-dimethyl 2'-aminophenoxo acetamide;2-(2-Amino-phenoxy)-N,N-dimethyl-acetamide;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-aminophenoxy)-N,N-dimethylacetamide

Chemical Property:

Melting Point:78 - 79 °C (toluene)
PSA：55.56000
LogP:1.31700

Purity/Quality:

Safty Information:

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Technology Process of 2-(2-aminophenoxy)-N,N-dimethylacetamide

There total 4 articles about 2-(2-aminophenoxy)-N,N-dimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 24011-73-2
N,N-dimetil-2-(2-nitrofenossi)acetammide

: 24011-74-3
N,N-dimetil-2-(2-amminofenossi)acetammide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1016/S0040-4020(00)00785-7

Reference yield:

: 1878-87-1
2-nitrophenoxyacetic acid

: 24011-74-3
N,N-dimetil-2-(2-amminofenossi)acetammide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 2 h / Heating

2: 1,2-dimethoxy-ethane / 4 h / Ambient temperature

3: 84.1 percent / hydrogen / 5percent Pd/C / tetrahydrofuran / 2660 Torr

With thionyl chloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,2-dimethoxyethane;

Reference yield:

: 20142-87-4
2-(2-nitrophenoxy)acetyl chloride

: 24011-74-3
N,N-dimetil-2-(2-amminofenossi)acetammide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2-dimethoxy-ethane / 4 h / Ambient temperature

2: 84.1 percent / hydrogen / 5percent Pd/C / tetrahydrofuran / 2660 Torr

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,2-dimethoxyethane;