Hydroperoxide, 1-aminocyclohexyl

Base Information

• Chemical Name: Hydroperoxide, 1-aminocyclohexyl
• CAS No.: 24075-24-9
• Molecular Formula: C6H13NO2
• Molecular Weight: 131.175

Synonyms:

Chemical Property of Hydroperoxide, 1-aminocyclohexyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hydroperoxide, 1-aminocyclohexyl

There total 1 articles about Hydroperoxide, 1-aminocyclohexyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 1-hydroperoxycyclohexylamine (24075-24-9)

Guidance literature:

With methanol; EDTA ; ammonia; dihydrogen peroxide;

DOI:10.1039/j39690002663

Reference yield: 90.0%

1-hydroperoxycyclohexylamine (24075-24-9) → cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4)

Guidance literature:

In acetonitrile; at 25 ℃; Inert atmosphere;

DOI:10.1021/jo302262a

Reference yield: 75.0%

1-hydroperoxycyclohexylamine (24075-24-9) → cyclohexanone-oxime (100-64-1) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4)

Guidance literature:

With tungsten trioxide; aluminum oxide; In acetonitrile; at 20 ℃; for 3h;

DOI:10.1002/anie.200705002

upstream raw materials:

cyclohexanone

Downstream raw materials:

N-(1-Acetylamino-cyclohexyl)-N-(1-hydroperoxy-cyclohexyl)-acetamide

cyclohexanone

1,1'-peroxy-dicyclohexylamine

cyclohexanone-oxime

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