2-Naphthaldehyde phenylhydrazone

Base Information

Chemical Name:2-Naphthaldehyde phenylhydrazone
CAS No.:24091-13-2
Molecular Formula:C17H14N2
Molecular Weight:246.312
Hs Code.:
European Community (EC) Number:661-906-5
Mol file:24091-13-2.mol

Synonyms:AKOS024339957;2-NAPHTHALDEHYDE PHENYLHYDRAZONE

Suppliers and Price of 2-Naphthaldehyde phenylhydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Naphthaldehyde phenylhydrazone

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:246.115698455
Heavy Atom Count:19
Complexity:294

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)NN=CC2=CC3=CC=CC=C3C=C2
Isomeric SMILES:C1=CC=C(C=C1)N/N=C/C2=CC3=CC=CC=C3C=C2

Technology Process of 2-Naphthaldehyde phenylhydrazone

There total 3 articles about 2-Naphthaldehyde phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 59-88-1
phenylhydrazine hydrochloride

: 66-99-9
β-naphthaldehyde

: 24091-13-2
1-(naphthalen-2-ylmethylene)-2-phenylhydrazine

Guidance literature:: With sodium acetate; In ethanol; at 80 ℃; for 0.0833333h; Microwave irradiation; air-cooling;
DOI:10.1021/co100015b

Reference yield:

: 62-53-3
aniline

: 24091-13-2
1-(naphthalen-2-ylmethylene)-2-phenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.25 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: sodium acetate / ethanol; water / 20 - 80 °C

With hydrogenchloride; sodium acetate; sodium nitrite; In ethanol; water;
DOI:10.1021/jo2005632