Technology Process of 5,9-Undecadienoic acid, 6,10-dimethyl-, (5E)-
There total 1 articles about 5,9-Undecadienoic acid, 6,10-dimethyl-, (5E)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 94 percent / DMPU / diethyl ether / 12 h / 20 °C
2.1: disiamylborane / tetrahydrofuran / 5.5 h / -10 °C
2.2: 72 percent / NaOH; 30 percent H2O2 / tetrahydrofuran; H2O / 18 h / 20 °C
3.1: 65 percent / Jones reagent / acetone / 3 h / 0 °C
With
1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; jones reagent; bis-(1,2-dimethylpropyl)borane;
In
tetrahydrofuran; diethyl ether; acetone;
DOI:10.1016/S0040-4020(01)01167-X
- Guidance literature:
-
With
tributylphosphine;
In
benzene;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: (i) NaH, benzene, (ii) oxalyl dichloride, (iii) /BRN= 102415/, Et2O, (iv) CuSO4, cyclohexane
2: NaH / 1,2-dimethoxy-ethane
3: NaBH4 / diethyl ether / 45 h / -20 °C
With
sodium tetrahydroborate; sodium hydride;
In
1,2-dimethoxyethane; diethyl ether;
DOI:10.1016/S0040-4039(01)88026-6
