Sn₂(N(H)C₆H₃-2,6-(i)Pr₂)3Cl

Base Information

• Chemical Name: Sn₂(N(H)C₆H₃-2,6-(i)Pr₂)3Cl
• CAS No.: 1093801-14-9
• Molecular Formula: C₃₆H₅₄ClN₃Sn₂
• Molecular Weight: 801.718
• Mol file: 1093801-14-9.mol

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Chemical Property of Sn₂(N(H)C₆H₃-2,6-(i)Pr₂)3Cl

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Technology Process of Sn₂(N(H)C₆H₃-2,6-(i)Pr₂)3Cl

There total 1 articles about Sn₂(N(H)C₆H₃-2,6-(i)Pr₂)3Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

lithium (2,6-diisopropylphenyl)amide + tin(ll) chloride → Sn2(N(H)C6H3-2,6-(i)Pr2)3Cl (1093801-14-9)

Guidance literature:

In diethyl ether; under inert atm. to suspn. SnCl2 in Et2O at 0°C soln. Li salt ligand in Et2O was added, stirred for 20 h at room temp.; volatiles were removed in vacuo, residue was extd. with hexane, filtered, and stored at -13°C for 3 days;

DOI:10.1039/b809671f