5-Phenyl-1,3-benzodioxole

Base Information

Chemical Name:5-Phenyl-1,3-benzodioxole
CAS No.:24382-05-6
Molecular Formula:C13H10O2
Molecular Weight:198.221
Hs Code.:
DSSTox Substance ID:DTXSID10573230
Nikkaji Number:J1.360.403G
Wikidata:Q82461855
Mol file:24382-05-6.mol

Synonyms:24382-05-6;5-Phenyl-1,3-benzodioxole;SCHEMBL404584;5-Phenyl-2H-1,3-benzodioxole;DTXSID10573230;AKOS006320849

Suppliers and Price of 5-Phenyl-1,3-benzodioxole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 5-Phenyl-1,3-benzodioxole

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:198.068079557
Heavy Atom Count:15
Complexity:211

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1OC2=C(O1)C=C(C=C2)C3=CC=CC=C3

Technology Process of 5-Phenyl-1,3-benzodioxole

There total 48 articles about 5-Phenyl-1,3-benzodioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2635-13-4
1,2-(methylenedioxy)-4-bromobenzene

: 98-80-6
phenylboronic acid

: 24382-05-6
3,4-methylenedioxybiphenyl

Guidance literature:: With palladium diacetate; N,N-diisopropyl-1,1-diphenylphosphanamine; potassium carbonate; In tetrahydrofuran; for 12h; Heating;
DOI:10.1016/S0040-4039(03)01743-X

Reference yield: 97.0%

: 7228-38-8
5-chloro-1,3-benzodioxole

: 2633-57-0
triallyl(phenyl)silane

: 24382-05-6
3,4-methylenedioxybiphenyl

Guidance literature:: triallyl(phenyl)silane; With tetrabutyl ammonium fluoride; In tetrahydrofuran; water; at 20 ℃; for 1h;

5-chloro-1,3-benzodioxole; With XPhos; bis(η3-allyl-μ-chloropalladium(II)); In tetrahydrofuran; water; at 80 ℃; for 14h;
DOI:10.1002/adsc.200404188

Reference yield: 96.0%

: 2635-13-4
1,2-(methylenedioxy)-4-bromobenzene

: 2633-57-0
triallyl(phenyl)silane

: 24382-05-6
3,4-methylenedioxybiphenyl

Guidance literature:: With tetrabutyl ammonium fluoride; palladium dichloride; tricyclohexylphosphine; In water; dimethyl sulfoxide; at 80 ℃; for 2h;
DOI:10.1016/j.jorganchem.2003.08.041