2-Cyclopenten-1-one, 2-(4-morpholinyl)-

Base Information

Chemical Name:2-Cyclopenten-1-one, 2-(4-morpholinyl)-
CAS No.:24454-33-9
Molecular Formula:C₉H₁₃NO₂
Molecular Weight:167.208
Hs Code.:
DSSTox Substance ID:DTXSID00484609
Nikkaji Number:J544.582E

Synonyms:2-Cyclopenten-1-one, 2-(4-morpholinyl)-;24454-33-9;morpholinocyclopent-2-en-1-one;DTXSID00484609

Suppliers and Price of 2-Cyclopenten-1-one, 2-(4-morpholinyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Cyclopenten-1-one, 2-(4-morpholinyl)-

Chemical Property:

XLogP3:0.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:167.094628657
Heavy Atom Count:12
Complexity:217

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC(=O)C(=C1)N2CCOCC2

Technology Process of 2-Cyclopenten-1-one, 2-(4-morpholinyl)-

There total 1 articles about 2-Cyclopenten-1-one, 2-(4-morpholinyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 936-52-7
1-(N-morpholino)cyclopent-1-ene

: 114336-39-9
3-benzenesulphonylcyclopent-2-en-1-one

: 132371-03-0
1α,2β,6β,7α-2-benzenesulphonyltricyclo<5.3.0.0^2.6>dec-8-ene-5-one

: 24454-33-9
2-morpholino-2-cyclopenten-1-one

Guidance literature:: With triethylamine; In benzene; at 20 ℃; for 24h;

Reference yield: 37.0%

: 24454-33-9
2-morpholino-2-cyclopenten-1-one

: 106-51-4
p-benzoquinone

: 103025-58-7
3-(2,5-Dihydroxyphenyl)-2-morpholino-2-cyclopenten-1-on

Guidance literature:: In acetic acid;

Reference yield:

: 24454-33-9
2-morpholino-2-cyclopenten-1-one

: C₁₅H₁₇NO₂

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2: caesium carbonate; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane; water / 1 h / 25 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; caesium carbonate; In 1,4-dioxane; dichloromethane; water; 2: |Suzuki Coupling;
DOI:10.1021/acs.orglett.8b00125