Pent-4-ene-1-sulfonamide

Base Information

Chemical Name:Pent-4-ene-1-sulfonamide
CAS No.:245368-50-7
Molecular Formula:C5H11NO2S
Molecular Weight:149.214
Hs Code.:
European Community (EC) Number:849-809-8
DSSTox Substance ID:DTXSID90472611
Nikkaji Number:J1.422.293F
Wikidata:Q82301606

Synonyms:Pent-4-ene-1-sulfonamide;245368-50-7;4-Pentene-1-sulfonamide;MFCD19382091;4-pentenylsulfonamide;SCHEMBL6300989;DTXSID90472611;GUYDOCPILYZNEK-UHFFFAOYSA-N;AKOS013585928;AS-57892;SY186295;CS-0139253;EN300-79869;C77524;Z1217214778

Suppliers and Price of Pent-4-ene-1-sulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Pent-4-ene-1-sulfonamide

Chemical Property:

XLogP3:0.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:149.05104977
Heavy Atom Count:9
Complexity:166

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCCCS(=O)(=O)N

Technology Process of Pent-4-ene-1-sulfonamide

There total 4 articles about Pent-4-ene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1119-51-3
bromopentene

: 245368-50-7
pent-4-ene-1-sulfonamide

Guidance literature:: bromopentene; With rongalite; In dimethyl sulfoxide; at 25 ℃; for 18h; Schlenk technique; Inert atmosphere;

With sodium acetate; hydroxylamine-O-sulfonic acid; In water; dimethyl sulfoxide; at 25 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.9b01732

Reference yield:

: 60154-77-0
pent-4-ene-1-sulfonyl chloride

: 245368-50-7
pent-4-ene-1-sulfonamide

Guidance literature:: With ammonium hydroxide; In acetonitrile;
DOI:10.1021/jo048990k

Reference yield:

: 1119-51-3
bromopentene

: 245368-50-7
pent-4-ene-1-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium sulphite / H₂O / Heating

1.2: phosphorous oxychloride / 130 °C

2.1: 0.820 g / aq. NH₃ / acetonitrile / 0 °C

With ammonium hydroxide; sodium sulfite; In water; acetonitrile; 1.1: Substitution / 1.2: Chlorination / 2.1: aminolysis;
DOI:10.1021/ol000130c