2-DECYLTHIOPHENE

Base Information

• Chemical Name: 2-DECYLTHIOPHENE
• CAS No.: 24769-39-9
• Molecular Formula: C14H24S
• Molecular Weight: 224.411
• Hs Code.: 2934999090
• Mol file: 24769-39-9.mol

Synonyms:Thiophene, 2-decyl-;Thiophene,2-decyl;2-(1-decyl)thiophene;2-Decanylthiophene;2-Decyl-thiophen;2-decyl-thiophene;2-n-decylthiophene;

Chemical Property of 2-DECYLTHIOPHENE

Chemical Property:

• Refractive Index: 1.4860 and le 1.4900
• Boiling Point: 167°C/17mmHg(lit.)
• PSA: 28.24000
• Density: 0.920±0.06 g/cm3(Predicted)
• LogP: 5.43130

Purity/Quality:

99% ^*data from raw suppliers

2-Decylthiophene >97.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-DECYLTHIOPHENE

There total 11 articles about 2-DECYLTHIOPHENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

thiophene (188290-36-0,8014-23-1,25233-34-5) + 1-bromo dodecane (112-29-8) → 2-decyl-thiophene (24769-39-9)

Guidance literature:

thiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

1-bromo dodecane; In tetrahydrofuran; hexane; at -78 - 20 ℃;

DOI:10.1016/j.molstruc.2008.12.039

Reference yield: 82.0%

thiophene (188290-36-0,8014-23-1,25233-34-5) + Iododecane (2050-77-3) → 2-decyl-thiophene (24769-39-9)

Guidance literature:

thiophene; With n-butyllithium; In hexane; at -78 ℃; for 1h;

Iododecane; In hexane; at -78 - 20 ℃;

DOI:10.1080/10587250108029957

Reference yield: 73.0%

2-bromothiophene (1003-09-4) + Iododecane (2050-77-3) → 2-decyl-thiophene (24769-39-9)

Guidance literature:

With pyridine; manganese; Tri(p-tolyl)phosphine; trifluoroacetic acid; cobalt(II) bromide; In N,N-dimethyl acetamide; at 70 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1002/ejoc.201500784

upstream raw materials:

2-Decanoylthiophene

thiophene

1-bromo dodecane

Iododecane

Downstream raw materials:

2-bromo-5-decylthiophene

palmitic acid

5-(5-decyl-[2]thienyl)-5-(2,4-dinitro-phenylhydrazono)-valeric acid ethyl ester

tricosanoic acid methyl ester

Refernces

• 1、 Allwright, Emily,Silber, Georg,Crain, Jason,Matsushita, Michio M.,Awaga, Kunio,Robertson, Neil. "Electrochemical deposition of highly-conducting metal dithiolene films". supporting information. p. 9363 - 9368. Retrieved 2016/06/14.
• 2、 -. "Use of compounds comprising a piperazine structural element in organic electronic devices and compounds and polymers comprising a piperazine structural element". Page/Page column. . Retrieved 2015/07/02.