3-Methyl-2-butenyl disulfide

Base Information

• Chemical Name: 3-Methyl-2-butenyl disulfide
• CAS No.: 24963-39-1
• Molecular Formula: C10H18S2
• Molecular Weight: 202.385
• UNII: PO7O52628V
• Nikkaji Number: J3.263.567I
• Mol file: 24963-39-1.mol

Synonyms:3-methyl-2-butenyl disulfide;Fema No. 4914;PO7O52628V;Bis -(3-methyl-2-butenyl)disulfide;UNII-PO7O52628V;24963-39-1;SCHEMBL7529589

Chemical Property of 3-Methyl-2-butenyl disulfide

Chemical Property:

• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 202.08499292
• Heavy Atom Count: 12
• Complexity: 141

Purity/Quality:

99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(=CCSSCC=C(C)C)C

Technology Process of 3-Methyl-2-butenyl disulfide

There total 2 articles about 3-Methyl-2-butenyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

ethanethioic acid S-(3-methyl-2-butenyl) ester (33049-93-3) → bis(3-methyl-2-buten-1-yl)disulfide (24963-39-1)

Guidance literature:

ethanethioic acid S-(3-methyl-2-butenyl) ester; With sodium methylate; In methanol; at 0 ℃; for 2h;

With iodine; In methanol; for 0.5h;

DOI:10.1080/17415993.2012.721368

Reference yield:

sodium phenoxide (139-02-6) + 2,2-dimethyl-3-(chloromethyl)thiirane → bis(3-methyl-2-buten-1-yl)disulfide (24963-39-1) + 2,2,-dimethyl-3-phenoxythietane

Guidance literature:

In ethanol; water; for 2h; Heating;

DOI:10.1023/A:1025592320130

upstream raw materials:

sodium phenoxide

ethanethioic acid S-(3-methyl-2-butenyl) ester