(+/-)-phthalic acid mono-(5,5-dimethyl-6-methylene-[2exo]norbornyl ester)

Base Information

• Chemical Name: (+/-)-phthalic acid mono-(5,5-dimethyl-6-methylene-[2exo]norbornyl ester)
• CAS No.: 99117-45-0
• Molecular Formula: C₁₈H₂₀O₄
• Molecular Weight: 300.354
• Mol file: 99117-45-0.mol

Synonyms:

Chemical Property of (+/-)-phthalic acid mono-(5,5-dimethyl-6-methylene-[2exo]norbornyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-phthalic acid mono-(5,5-dimethyl-6-methylene-[2exo]norbornyl ester)

There total 3 articles about (+/-)-phthalic acid mono-(5,5-dimethyl-6-methylene-[2exo]norbornyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dl-camphene (565-00-4) → (+/-)-phthalic acid mono-(5,5-dimethyl-6-methylene-[2exo]norbornyl ester) (99117-45-0)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrachloromethane; sodium hydrogencarbonate; potassium permanganate / Reagens 4: konz. wss. Salzsaeure; Erhitzen des Reaktionsprodukts mit Essigsaeure und Kaliumacetat und Behandeln des danach isolierten Reaktionsprodukts mit aethanol. Kalilauge

With tetrachloromethane; potassium permanganate; sodium hydrogencarbonate;

Reference yield:

→ Camphenol-(6)-hydrogenphthalat (99117-45-0)

Guidance literature:

Camphenol-(6), Phthalsaeureanhydrid, Py.;

DOI:10.1021/jo01033a522

Reference yield:

phthalic anhydride (85-44-9) + exo-2,2-dimethyl-3-methylenebicyclo<2.2.1>heptan-5-ol (54672-39-8) → (+/-)-phthalic acid mono-(5,5-dimethyl-6-methylene-[2exo]norbornyl ester) (99117-45-0)

Guidance literature:

upstream raw materials:

phthalic anhydride

exo-2,2-dimethyl-3-methylenebicyclo<2.2.1>heptan-5-ol

dl-camphene