Cyclohexanol, 4-(1,1-dimethylethyl)-1-ethyl-, trans-

Base Information

• Chemical Name: Cyclohexanol, 4-(1,1-dimethylethyl)-1-ethyl-, trans-
• CAS No.: 25143-76-4
• Molecular Formula: C12H24O
• Molecular Weight: 184.322
• Mol file: 25143-76-4.mol

Synonyms:

Chemical Property of Cyclohexanol, 4-(1,1-dimethylethyl)-1-ethyl-, trans-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanol, 4-(1,1-dimethylethyl)-1-ethyl-, trans-

There total 12 articles about Cyclohexanol, 4-(1,1-dimethylethyl)-1-ethyl-, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-tert-Butyl-1-(1-methylselanyl-ethyl)-cyclohexanol (94718-84-0) → trans-4-t-butyl-1-ethyl-1-cyclohexanol (25143-76-4)

Guidance literature:

With lithium; ethylamine; at -15 ℃; for 2h;

Reference yield: 91.0%

ethylmagnesium bromide (925-90-6) + 4-tercbutyl-cyclohexanone (98-53-3) → trans-4-t-butyl-1-ethyl-1-cyclohexanol (25143-76-4)

Guidance literature:

With methylaluminum bis(2,6-di-tert-butylphenoxide); In diethyl ether; toluene; at -78 ℃; for 2h;

DOI:10.1021/ja00219a038

Reference yield: 54.0%

cis-7-tert-butyl-1-oxaspiro<3.5>nonane (72091-16-8) → trans-4-t-butyl-1-ethyl-1-cyclohexanol (25143-76-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 64h; Product distribution; Heating; other reagent, reaction time, solvent;

DOI:10.1021/ja00340a019

upstream raw materials:

1-ethynyl-t-4-tert-butylcyclohexan-r-1-ol

ethylmagnesium bromide

4-tercbutyl-cyclohexanone

methylenebis(diethylalane)