3-Methyl-3-buten-1-ol, TMS derivative

Base Information

Chemical Name:3-Methyl-3-buten-1-ol, TMS derivative
CAS No.:25195-89-5
Molecular Formula:C8H18OSi
Molecular Weight:158.316
Hs Code.:
DSSTox Substance ID:DTXSID201260621
Nikkaji Number:J2.209.412B
Mol file:25195-89-5.mol

Synonyms:3-Methyl-3-buten-1-ol, TMS derivative;JHTHPYMRROBKBP-UHFFFAOYSA-N;DTXSID201260621;25195-89-5;3-Methyl-3-buten-1-ol, trimethylsilyl ether;Trimethyl[(3-methyl-3-buten-1-yl)oxy]silane;Trimethyl[(3-methylbut-3-en-1-yl)oxy]silane #

Suppliers and Price of 3-Methyl-3-buten-1-ol, TMS derivative

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Methyl-3-buten-1-ol, TMS derivative

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:158.112691728
Heavy Atom Count:10
Complexity:113

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=C)CCO[Si](C)(C)C

Technology Process of 3-Methyl-3-buten-1-ol, TMS derivative

There total 1 articles about 3-Methyl-3-buten-1-ol, TMS derivative which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6245-99-4
2,2-dimethyl-oxetane

: 3908-55-2
Trimethyl(methylthio)silane

: 25195-89-5
(3-methylbut-3-en-1-oxy)trimethylsilane

: (4-methylthio-2-methyl-2-butoxy)trimethylsilane

: (3-methylthio-3-methylbutoxy)trimethylsilane

Guidance literature:: With zinc(II) chloride; In 1,2-dichloro-ethane; at 70 ℃; for 21h;
DOI:10.1016/S0022-328X(00)89147-0

Reference yield: 53.0%

: 25195-89-5
(3-methylbut-3-en-1-oxy)trimethylsilane

: 103-79-7,136675-26-8
1-phenyl-acetone

: 1,9-dimethyl-10-oxatricyclo[7.3.1.02,7]-trideca-2,4,6-triene

: 1,9-dimethyl-10-oxatricyclo[7.3.1.02,7]-trideca-2,4,6-triene

: C₁₄H₁₈O

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; Reflux;
DOI:10.1021/jo501755x

Reference yield: 21.0%

: 1444-65-1
(RS)-2-phenylcyclohexanone

: 25195-89-5
(3-methylbut-3-en-1-oxy)trimethylsilane

: 4-methyl-7-phenyl-1-oxaspiro[5.5]undec-4-ene

: 4-methyl-7-phenyl-1-oxaspiro[5.5]undec-4-ene

: 4-methyl-7-phenyl-1-oxaspiro[5.5]undec-3-ene

: 1-methyl-14-oxatetracyclo[11.3.1.02,7.08,13]heptadeca-2,4,6-triene

Guidance literature:: (RS)-2-phenylcyclohexanone; (3-methylbut-3-en-1-oxy)trimethylsilane; In dichloromethane; at -20 ℃; for 0.0833333h; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 4h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo501755x