{Mo(CO)5(CNHC₆H₄C(P(C₆H₅)3))}

Base Information

• Chemical Name: {Mo(CO)5(CNHC₆H₄C(P(C₆H₅)3))}
• CAS No.: 146596-86-3
• Molecular Formula: C₃₁H₂₀MoNO₅P
• Molecular Weight: 613.417

Synonyms:

Chemical Property of {Mo(CO)5(CNHC₆H₄C(P(C₆H₅)3))}

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of {Mo(CO)5(CNHC₆H₄C(P(C₆H₅)3))}

There total 1 articles about {Mo(CO)5(CNHC₆H₄C(P(C₆H₅)3))} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{Mo(CO)5((C6H5)3PCH2C6H4NC)}(1+)*BF4(1-)={Mo(CO)5((C6H5)3PCH2C6H4NC)}{BF4} + sodium hexamethyldisilazane (1070-89-9) → {Mo(CO)5(CNH2C6H4C(P(C6H5)3))}(1+)*BF4(1-)={Mo(CO)5(CNH2C6H4C(P(C6H5)3))}BF4 + {Mo(CO)5(CNHC6H4C(P(C6H5)3))} (146596-86-3)

Guidance literature:

In tetrahydrofuran; byproducts: NH(SiMe3)2, NaBF4; react. under N2, dropwise add. of Na(N(SiMe3)2) in THF to a suspension of (Mo(CO)5(o-Ph3PCH2C6H4CN))(BF4) in THF at -40°C, stirring for 30 min at this temp., stirring at room temp. for 1.5 h; evapg. to dryness under vac., washing with water, dissolving in CH2Cl2, drying over anhyd. Na2SO4, filtration, evapg. under reduced pressure, washing with pentane, filtration, drying under vac., not seperated, determination by NMR spectroscopy;

DOI:10.1039/DT9920002827

Reference yield:

tetrafluoroboric acid diethyletherate + {Mo(CO)5(CNHC6H4C(P(C6H5)3))} (146596-86-3) → {Mo(CO)5(CNH2C6H4C(P(C6H5)3))}(1+)*BF4(1-)={Mo(CO)5(CNH2C6H4C(P(C6H5)3))}BF4

Guidance literature:

In acetonitrile; generating the complex in situ by addn. of (Et2OH)BF4 to the indole complex; not isolated;

DOI:10.1039/DT9920002827

upstream raw materials:

sodium hexamethyldisilazane

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