tert-Butyl-{(3aR,5R,6S,6aR)-2,2-dimethyl-5-[(E)-2-((4R,6R)-6-methyl-4-phenylsulfanyl-5,6-dihydro-4H-pyran-2-yl)-vinyl]-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy}-diphenyl-silane

Base Information

• Chemical Name: tert-Butyl-{(3aR,5R,6S,6aR)-2,2-dimethyl-5-[(E)-2-((4R,6R)-6-methyl-4-phenylsulfanyl-5,6-dihydro-4H-pyran-2-yl)-vinyl]-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy}-diphenyl-silane
• CAS No.: 137166-24-6
• Molecular Formula: C₃₇H₄₄O₅SSi
• Molecular Weight: 628.905

Synonyms:

Chemical Property of tert-Butyl-{(3aR,5R,6S,6aR)-2,2-dimethyl-5-[(E)-2-((4R,6R)-6-methyl-4-phenylsulfanyl-5,6-dihydro-4H-pyran-2-yl)-vinyl]-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy}-diphenyl-silane

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Technology Process of tert-Butyl-{(3aR,5R,6S,6aR)-2,2-dimethyl-5-[(E)-2-((4R,6R)-6-methyl-4-phenylsulfanyl-5,6-dihydro-4H-pyran-2-yl)-vinyl]-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy}-diphenyl-silane

There total 2 articles about tert-Butyl-{(3aR,5R,6S,6aR)-2,2-dimethyl-5-[(E)-2-((4R,6R)-6-methyl-4-phenylsulfanyl-5,6-dihydro-4H-pyran-2-yl)-vinyl]-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy}-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2R,6R)-2-Methyl-6-phenylsulfanyl-3,6-dihydro-2H-pyran (137166-21-3) + tert-Butyl-[(3aR,5S,6S,6aR)-5-(2,2-dioxo-2λ6-[1,3,2]dioxathiolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-diphenyl-silane (137166-23-5) → tert-Butyl-{(3aR,5R,6S,6aR)-2,2-dimethyl-5-[(E)-2-((4R,6R)-6-methyl-4-phenylsulfanyl-5,6-dihydro-4H-pyran-2-yl)-vinyl]-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy}-diphenyl-silane (137166-24-6)

Guidance literature:

With n-butyllithium; sulfuric acid; water;

DOI:10.1039/c39910001207

Reference yield:

(2R,6R)-2-Methyl-6-phenylsulfanyl-3,6-dihydro-2H-pyran (137166-21-3) + tert-Butyl-[(3aR,5S,6S,6aR)-5-(2,2-dioxo-2λ6-[1,3,2]dioxathiolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-diphenyl-silane (137166-23-5) → (R)-1-[(3aR,5R,6S,6aR)-6-(tert-Butyl-diphenyl-silanyloxy)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl]-2-((4R,6R)-6-methyl-4-phenylsulfanyl-5,6-dihydro-4H-pyran-2-yl)-ethanol (137166-25-7) + tert-Butyl-{(3aR,5R,6S,6aR)-2,2-dimethyl-5-[(E)-2-((4R,6R)-6-methyl-4-phenylsulfanyl-5,6-dihydro-4H-pyran-2-yl)-vinyl]-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy}-diphenyl-silane (137166-24-6)

Guidance literature:

With n-butyllithium; sulfuric acid; water;

DOI:10.1039/c39910001207

upstream raw materials:

(2R,6R)-2-Methyl-6-phenylsulfanyl-3,6-dihydro-2H-pyran

tert-Butyl-[(3aR,5S,6S,6aR)-5-(2,2-dioxo-2λ⁶-[1,3,2]dioxathiolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-diphenyl-silane

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