1,5,6,7,8,8a-Hexahydro-2,5,5,8aα-tetramethyl-1β,6β-methanonaphthalene-4aα(4H)-ol

Base Information

Chemical Name:1,5,6,7,8,8a-Hexahydro-2,5,5,8aα-tetramethyl-1β,6β-methanonaphthalene-4aα(4H)-ol
CAS No.:17806-54-1
Molecular Formula:C₁₅H₂₄O
Molecular Weight:220.355
Hs Code.:
Mol file:17806-54-1.mol

Synonyms:1,6-Methanonaphthalen-1(2H)-ol,4a,5,6,7,8,8a-hexahydro-4,8a,9,9-tetramethyl-, [1R-(1a,4aa,6b,8aa)]-; Patchenol; Patchoulenol

Suppliers and Price of 1,5,6,7,8,8a-Hexahydro-2,5,5,8aα-tetramethyl-1β,6β-methanonaphthalene-4aα(4H)-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 1,5,6,7,8,8a-Hexahydro-2,5,5,8aα-tetramethyl-1β,6β-methanonaphthalene-4aα(4H)-ol

Chemical Property:

PSA：20.23000
LogP:3.52990

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1,5,6,7,8,8a-Hexahydro-2,5,5,8aα-tetramethyl-1β,6β-methanonaphthalene-4aα(4H)-ol

There total 9 articles about 1,5,6,7,8,8a-Hexahydro-2,5,5,8aα-tetramethyl-1β,6β-methanonaphthalene-4aα(4H)-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 77584-09-9,77646-45-8
(1R,4S,6S)-6-((S)-1-Methoxymethoxy-1-methyl-allyl)-1,3,3-trimethyl-bicyclo[2.2.2]octan-2-one

: 17806-54-1,77584-13-5
(4aR,6S,8aR)-4,8a,9,9-Tetramethyl-4a,5,6,7,8,8a-hexahydro-2H-1,6-methano-naphthalen-1-ol

Guidance literature:: sodium; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)71484-5

Reference yield:

: 1125-21-9
2,6,6-trimethyl-2-cyclohexene-1,4-dione

: 17806-54-1,77584-13-5
(4aR,6S,8aR)-4,8a,9,9-Tetramethyl-4a,5,6,7,8,8a-hexahydro-2H-1,6-methano-naphthalen-1-ol

Guidance literature:: Multi-step reaction with 9 steps

1: N₂H₄

2: MnO₂

3: CuSO₄ / Heating

4: 96 percent / 200 °C

5: 95 percent / hydrogene / Pd/C / 20 °C

6: 70 percent / CH₃ONa / methanol

8: 97 percent / acetonitrile / Heating

9: 64 percent / Na / tetrahydrofuran

With manganese(IV) oxide; hydrogen; sodium methylate; copper(II) sulfate; hydrazine; palladium on activated charcoal; sodium; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1016/S0040-4039(00)71484-5

Reference yield:

: 13487-30-4
2,6,6-trimethylcyclohexa-2,4-dienone

: 17806-54-1,77584-13-5
(4aR,6S,8aR)-4,8a,9,9-Tetramethyl-4a,5,6,7,8,8a-hexahydro-2H-1,6-methano-naphthalen-1-ol

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / 200 °C

2: 95 percent / hydrogene / Pd/C / 20 °C

3: 70 percent / CH₃ONa / methanol

5: 97 percent / acetonitrile / Heating

6: 64 percent / Na / tetrahydrofuran

With hydrogen; sodium methylate; palladium on activated charcoal; sodium; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1016/S0040-4039(00)71484-5