(PrCl₂(((H₃C)2N)3PO)4)⁽¹⁺⁾*B(C₆H₅)4^(1-)=(PrCl₂(((H₃C)2N)3PO)4)(B(C₆H₅)4)

Base Information

• Chemical Name: (PrCl₂(((H₃C)2N)3PO)4)⁽¹⁺⁾*B(C₆H₅)4^(1-)=(PrCl₂(((H₃C)2N)3PO)4)(B(C₆H₅)4)
• CAS No.: 109181-26-2
• Molecular Formula: C₂₄H₂₀B*C₂₄H₇₂Cl₂N₁₂O₄P₄Pr
• Molecular Weight: 1247.86
• Mol file: 109181-26-2.mol

Synonyms:

Chemical Property of (PrCl₂(((H₃C)2N)3PO)4)⁽¹⁺⁾*B(C₆H₅)4^(1-)=(PrCl₂(((H₃C)2N)3PO)4)(B(C₆H₅)4)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (PrCl₂(((H₃C)2N)3PO)4)⁽¹⁺⁾*B(C₆H₅)4^(1-)=(PrCl₂(((H₃C)2N)3PO)4)(B(C₆H₅)4)

There total 1 articles about (PrCl₂(((H₃C)2N)3PO)4)⁽¹⁺⁾*B(C₆H₅)4^(1-)=(PrCl₂(((H₃C)2N)3PO)4)(B(C₆H₅)4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N,N,N,N,N-hexamethylphosphoric triamide (680-31-9) + praseodymium(III) chloride hydrate (10025-90-8,17272-46-7,19423-77-9) + sodium tetraphenyl borate (143-66-8) → (PrCl2(((H3C)2N)3PO)4)(1+)*B(C6H5)4(1-)=(PrCl2(((H3C)2N)3PO)4)(B(C6H5)4) (109181-26-2)

Guidance literature:

In acetone; byproducts: NaCl; PrCl3*99H2O is dissolved in acetone under heating in presence of ethyl orthoformate and the stoichiometric amt. of TDMPO. A soln. of NaBPh4 in acetone is added to the cooled soln.; After 1 h the NaCl ppt. is filtered and the filtrate is evapd. After redissolution and filtration the dichloride complex is pptd. by slow addn.of diethyl ether, sepd., washed twice with diethyl ether and dried in vacuo over CaCl2. Elem. anal.;

upstream raw materials:

N,N,N,N,N,N-hexamethylphosphoric triamide

praseodymium(III) chloride hydrate

sodium tetraphenyl borate