1,4,7-Trifluoro-2-nitro-9h-fluoren-9-one

Base Information

Chemical Name:1,4,7-Trifluoro-2-nitro-9h-fluoren-9-one
CAS No.:17698-83-8
Molecular Formula:C₁₃H₄F₃NO₃
Molecular Weight:279.175
Hs Code.:
NSC Number:98121
DSSTox Substance ID:DTXSID40294789
Wikidata:Q82034297

Synonyms:17698-83-8;1,4,7-trifluoro-2-nitro-9h-fluoren-9-one;NSC98121;NCIOpen2_006344;DTXSID40294789;NSC-98121

Suppliers and Price of 1,4,7-Trifluoro-2-nitro-9h-fluoren-9-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,4,7-Trifluoro-2-nitro-9h-fluoren-9-one

Chemical Property:

Vapor Pressure:9.41E-09mmHg at 25°C
Boiling Point:463°C at 760 mmHg
Flash Point:233.8°C
Density:1.648g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:0
Exact Mass:279.01432748
Heavy Atom Count:20
Complexity:441

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C(C=C1F)C(=O)C3=C(C(=CC(=C23)F)[N+](=O)[O-])F

Technology Process of 1,4,7-Trifluoro-2-nitro-9h-fluoren-9-one

There total 11 articles about 1,4,7-Trifluoro-2-nitro-9h-fluoren-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17532-99-9
1,4,7-Trifluor-fluoren-9-on

: 17698-83-8
1,4,7-Trifluor-2-nitro-fluoren-9-on

Guidance literature:: With nitric acid;
DOI:10.1139/v67-418

Reference yield:

: 2265-92-1
1,4-difluoro-2-iodobenzene

: 17698-83-8
1,4,7-Trifluor-2-nitro-fluoren-9-on

Guidance literature:: Multi-step reaction with 5 steps

1: Cu / 200 °C

2: HNO₃

3: SnCl₂*2H₂O, aq. HCl

4: (i) NaNO₂, aq. HBF₄, (ii) (thermolysis)

5: HNO₃

With hydrogenchloride; nitric acid; copper; tin(ll) chloride;
DOI:10.1139/v67-418

Reference yield:

: 17532-94-4
1,4-difluoro-9-fluorenone

: 17698-83-8
1,4,7-Trifluor-2-nitro-fluoren-9-on

Guidance literature:: Multi-step reaction with 4 steps

1: HNO₃

2: SnCl₂*2H₂O, aq. HCl

3: (i) NaNO₂, aq. HBF₄, (ii) (thermolysis)

4: HNO₃

With hydrogenchloride; nitric acid; tin(ll) chloride;
DOI:10.1139/v67-418