Phosphine, tris[3-(trifluoromethyl)phenyl]-

Base Information

Chemical Name:Phosphine, tris[3-(trifluoromethyl)phenyl]-
CAS No.:25688-46-4
Molecular Formula:C21H12F9P
Molecular Weight:466.286
Hs Code.:
Mol file:25688-46-4.mol

Synonyms:tris<3-(trifluoromethyl)phenyl>tris(3-trifluoromethylphenyl)-phosphine;tris-(3-(trifluoromethyl)phenyl)phosphane;Phosphine,tris[3-(trifluoromethyl)phenyl];3-(trifluormethyl)phenyl>CTK0J3840;tri(m-trifluoromethylphenyl)-phosphine;Tris-(m-trifluoromethylphenyl)phosphine;

Suppliers and Price of Phosphine, tris[3-(trifluoromethyl)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Phosphine, tris[3-(trifluoromethyl)phenyl]-

Chemical Property:

Boiling Point:340 °C
PSA：13.59000
LogP:6.50120

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phosphine, tris[3-(trifluoromethyl)phenyl]-

There total 3 articles about Phosphine, tris[3-(trifluoromethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 401-78-5
3-bromo-1-trifluoromethylbenzene

: 25688-46-4
tris(3-trifluoromethylphenyl)-phosphine

Guidance literature:: 3-bromo-1-trifluoromethylbenzene; With magnesium; In diethyl ether; for 2h; Reflux; Schlenk technique; Inert atmosphere;

With phosphorus trichloride; In diethyl ether; at 0 ℃; for 1h; Reflux; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejic.202000887

Reference yield:

: 401-81-0
m-trifluoromethylphenyl iodide

: 25688-46-4
tris(3-trifluoromethylphenyl)-phosphine

: tetra(m-benzotrifluoride)phosphonium iodide

Guidance literature:: With dihydrogen phosphide sodium; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; triethylamine; In acetonitrile; at 20 ℃; for 24h; Reagent/catalyst; Sealed tube; Irradiation; Schlenk technique; Glovebox; Inert atmosphere;
DOI:10.1002/anie.202110619