dithiocyanatobis(1-benzyl-2-(naphthyl-β-azo)imidazole)manganese(II)

Base Information

• Chemical Name: dithiocyanatobis(1-benzyl-2-(naphthyl-β-azo)imidazole)manganese(II)
• CAS No.: 955946-89-1
• Molecular Formula: C₄₂H₃₂MnN₁₀S₂
• Molecular Weight: 795.853
• Mol file: 955946-89-1.mol

Synonyms:

Chemical Property of dithiocyanatobis(1-benzyl-2-(naphthyl-β-azo)imidazole)manganese(II)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dithiocyanatobis(1-benzyl-2-(naphthyl-β-azo)imidazole)manganese(II)

There total 1 articles about dithiocyanatobis(1-benzyl-2-(naphthyl-β-azo)imidazole)manganese(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ammonium thiocyanate + manganese(II) perchlorate hexahydrate + 1-benzyl-2-(naphthyl-β-azo)-imidazole (295806-51-8) → dithiocyanatobis(1-benzyl-2-(naphthyl-β-azo)imidazole)manganese(II) (955946-89-1)

Guidance literature:

In methanol; Mn salt in MeOH added dropwise to MeOH soln. of ligand at 298 K; stirredfor 15 min; filtered; NaSCN in MeOH added to filtrate; kept undisturbed for a few d; filtered; ppt. washed with cold H2O and MeOH; dried in vac. over silica gel; elem. anal.;

DOI:10.1016/j.molstruc.2006.11.076

upstream raw materials:

1-benzyl-2-(naphthyl-β-azo)-imidazole