2,2,9,9-tetramethyl-decanedioic acid-dianilide

Base Information

• Chemical Name: 2,2,9,9-tetramethyl-decanedioic acid-dianilide
• CAS No.: 124135-73-5
• Molecular Formula: C₂₆H₃₆N₂O₂
• Molecular Weight: 408.584
• Mol file: 124135-73-5.mol

Synonyms:

Chemical Property of 2,2,9,9-tetramethyl-decanedioic acid-dianilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2,9,9-tetramethyl-decanedioic acid-dianilide

There total 4 articles about 2,2,9,9-tetramethyl-decanedioic acid-dianilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-methoxy-5,5-dimethyl-6-oxohexanoic acid (86178-22-5) → 2,2,9,9-tetramethyl-decanedioic acid-dianilide (124135-73-5)

Guidance literature:

Multi-step reaction with 3 steps

1: methanol / Electrolysis

2: aq.-ethanolic KOH-solution

3: acetyl chloride / anschliessend mit Anilin

With methanol; potassium hydroxide; acetyl chloride;

Reference yield:

dimethyl 1,1-dimethyladipate (17219-21-5) → 2,2,9,9-tetramethyl-decanedioic acid-dianilide (124135-73-5)

Guidance literature:

Multi-step reaction with 4 steps

1: methanol. KOH-solution

2: methanol / Electrolysis

3: aq.-ethanolic KOH-solution

4: acetyl chloride / anschliessend mit Anilin

With methanol; potassium hydroxide; acetyl chloride;

Reference yield:

2,2,9,9-tetramethyl-decanedioic acid dimethyl ester (22092-66-6) → 2,2,9,9-tetramethyl-decanedioic acid-dianilide (124135-73-5)

Guidance literature:

Multi-step reaction with 2 steps

1: aq.-ethanolic KOH-solution

2: acetyl chloride / anschliessend mit Anilin

With potassium hydroxide; acetyl chloride;

upstream raw materials:

2,2,9,9-tetramethyl-decanedioic acid

6-methoxy-5,5-dimethyl-6-oxohexanoic acid

dimethyl 1,1-dimethyladipate

2,2,9,9-tetramethyl-decanedioic acid dimethyl ester