methyl N-hexanoylglycinate

Base Information

• Chemical Name: methyl N-hexanoylglycinate
• CAS No.: 31295-09-7
• Molecular Formula: C₉H₁₇NO₃
• Molecular Weight: 187.239
• Mol file: 31295-09-7.mol

Synonyms:Glycine,N-hexanoyl-, methyl ester (8CI); Methyl N-hexanoylglycinate;N-n-Hexanoylglycine methyl ester; NSC 359574

Chemical Property of methyl N-hexanoylglycinate

Chemical Property:

• Vapor Pressure: 0.00084mmHg at 25°C
• Boiling Point: 305.1°C at 760 mmHg
• Flash Point: 138.3°C
• Density: 1.003g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl N-hexanoylglycinate

There total 2 articles about methyl N-hexanoylglycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

glycine ethyl ester hydrochloride (5680-79-5,883886-67-7) + hexanal (66-25-1) → N-hexanoylglycine methyl ester (31295-09-7)

Guidance literature:

With tert.-butylhydroperoxide; copper(ll) sulfate pentahydrate; calcium carbonate; In water; acetonitrile; at 20 ℃; Inert atmosphere;

DOI:10.1021/jo301252c DOI:10.1021/jo301252c

Reference yield:

dimethylsulfite (616-42-2) + N-hexanoylglycine (24003-67-6) → N-hexanoylglycine methyl ester (31295-09-7)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

dimethylsulfite

N-hexanoylglycine

glycine ethyl ester hydrochloride

hexanal