dicarbonyl(η5-cyclopentadienyl)(trimethylphosphine)(diphenylphosphine)tungsten(II) tetrafluoroborate

Base Information

• Chemical Name: dicarbonyl(η5-cyclopentadienyl)(trimethylphosphine)(diphenylphosphine)tungsten(II) tetrafluoroborate
• CAS No.: 99394-96-4
• Molecular Formula: BF₄*C₂₂H₂₅O₂P₂W
• Molecular Weight: 654.041

Synonyms:

Chemical Property of dicarbonyl(η5-cyclopentadienyl)(trimethylphosphine)(diphenylphosphine)tungsten(II) tetrafluoroborate

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Technology Process of dicarbonyl(η5-cyclopentadienyl)(trimethylphosphine)(diphenylphosphine)tungsten(II) tetrafluoroborate

There total 1 articles about dicarbonyl(η5-cyclopentadienyl)(trimethylphosphine)(diphenylphosphine)tungsten(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(C5H5)(CO)2W(P(CH3)3)P(C6H5)2 → dicarbonyl(η5-cyclopentadienyl)(trimethylphosphine)(diphenylphosphine)tungsten(II) tetrafluoroborate (99394-96-4)

Guidance literature:

With boron trifluoride etherate; In toluene; a toluene soln. of BF3*OEt2 was added dropwise at room temp. to a soln.of W-complex in toluene, mixt. was stirred for 3 h; ppt. was sepd., repeatedly washed with pentane, dried in vacuo;

DOI:10.1016/0022-328X(85)88016-5

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