2,2'-[(2-Hydroxy-1,3-phenylene)bis(methylene)]diphenol

Base Information

• Chemical Name: 2,2'-[(2-Hydroxy-1,3-phenylene)bis(methylene)]diphenol
• CAS No.: 2677-32-9
• Molecular Formula: C20H18O3
• Molecular Weight: 306.361
• ChEMBL ID: CHEMBL117392
• DSSTox Substance ID: DTXSID10497184
• Nikkaji Number: J3.512.316D

Synonyms:2677-32-9;SCHEMBL54577;CHEMBL117392;2,2'-[(2-Hydroxy-1,3-phenylene)bis(methylene)]diphenol;DTXSID10497184;2,6-bis-(o-Hydroxybenzyl)-phenol

Chemical Property of 2,2'-[(2-Hydroxy-1,3-phenylene)bis(methylene)]diphenol

Chemical Property:

• XLogP3: 4.7
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 306.125594432
• Heavy Atom Count: 23
• Complexity: 327

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)CC2=C(C(=CC=C2)CC3=CC=CC=C3O)O)O

Technology Process of 2,2'-[(2-Hydroxy-1,3-phenylene)bis(methylene)]diphenol

There total 9 articles about 2,2'-[(2-Hydroxy-1,3-phenylene)bis(methylene)]diphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,6-bis(hydroxymethyl)phenol (2937-59-9) + phenol (108-95-2,27073-41-2) → 2,6-Bis-(2-hydroxy-benzyl)-phenol (2677-32-9)

Guidance literature:

With sulfonated multi-walled carbon nanotubes; In neat (no solvent); at 110 ℃; for 0.333333h; Catalytic behavior;

DOI:10.1039/c5nj03136b

Reference yield: 88.0%

4-bromo-2,6-bis(5'-bromo-2'-hydroxy-α-tolyl)phenol (35280-40-1) → 2,6-Bis-(2-hydroxy-benzyl)-phenol (2677-32-9)

Guidance literature:

With potassium hydroxide; zinc; for 4h; Heating;

DOI:10.1002/hlca.19810640224

Reference yield:

4-chloro-2,6-bis(5-chloro-2-hydroxybenzyl)phenol (6642-07-5) → 2,6-Bis-(2-hydroxy-benzyl)-phenol (2677-32-9)

Guidance literature:

With sodium hydroxide; aluminum nickel;

DOI:10.1007/BF00903009

upstream raw materials:

Bis(2-hydroxyphenyl)methane

salicylic alcohol

4-chloro-2,6-bis(5-chloro-2-hydroxybenzyl)phenol

2,6-bis(hydroxymethyl)phenol

Downstream raw materials:

2,6-Bis-(2-hydroxy-5-phenylazo-benzyl)-4-phenylazo-phenol

2,6-di(o-anisyl)anisole

25,26,27,28-tetrakis(hydroxy)calix[4]arene

triphenoxyacetic acid

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