tris-(N-methylindol-3-yl)methane

Base Information

• Chemical Name: tris-(N-methylindol-3-yl)methane
• CAS No.: 27065-95-8
• Molecular Formula: C28H25N3
• Molecular Weight: 403.527
• Mol file: 27065-95-8.mol

Synonyms:tris(1-methyl-1H-indol-3-yl)methane;Tris-(1-methyl-3-indolyl)methan;tris-(N-methylindol-3-yl)methane;tris(1-methyl-3-indolyl)methane;tris(1-methylindol-3-yl)methane;tris-(1-methylindol-3-yl)methane;

Chemical Property of tris-(N-methylindol-3-yl)methane

Chemical Property:

• Melting Point: 223 °C
• Boiling Point: 627.8±50.0 °C(Predicted)
• PSA: 14.79000
• Density: 1.18±0.1 g/cm3(Predicted)
• LogP: 6.34190

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tris-(N-methylindol-3-yl)methane

There total 2 articles about tris-(N-methylindol-3-yl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

1-methylindole (603-76-9) + Indole-3-carboxaldehyde (487-89-8,1228547-52-1) → indole (120-72-9) + tris(1-methyl-1H-indol-3-yl)methane (27065-95-8)

Guidance literature:

With ammonium chloride; at 120 ℃; for 3h; neat (no solvent);

DOI:10.3184/030823408X361101

Reference yield: 12.0%

1-methylindole (603-76-9) + Indole-3-carboxaldehyde (487-89-8,1228547-52-1) → indole (120-72-9) + tris(1-methyl-1H-indol-3-yl)methane (27065-95-8) + 3,3'-[(1-methyl-1H-indol-3-yl)methylene]bis(1H-indole) + 3,3'-[(1H-indol-3-yl)methylene]bis(1-methyl-1H-indole)

Guidance literature:

With Montmorillonite K₁₀; In methanol; ethyl acetate; at 20 ℃; for 0.0833333h;

DOI:10.1016/S0040-4039(01)02380-2

upstream raw materials:

1-methylindole

Indole-3-carboxaldehyde

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