5,6-Dihydro-6-oxophenanthridine-3-carboxylic acid

Base Information

Chemical Name:5,6-Dihydro-6-oxophenanthridine-3-carboxylic acid
CAS No.:39161-52-9
Molecular Formula:C₁₄H₉NO₃
Molecular Weight:239.23
Hs Code.:
Mol file:39161-52-9.mol

Synonyms:6-oxo-5,6-dihydrophenanthridine-3-carboxylic acid;5,6-Dihydro-6-oxophenanthridine-3-carboxylic acid;5[H]phenanthridin-6-one carboxylic acid;Acido 6-fenantridon-3-carbossilico [Italian];Phenanthridine-3-carboxylic acid,5,6-dihydro-6-oxo;6-Phenanthridon-3-carbonsaeure;

Suppliers and Price of 5,6-Dihydro-6-oxophenanthridine-3-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 5,6-Dihydro-6-oxophenanthridine-3-carboxylic acid

Chemical Property:

Vapor Pressure:9.21E-07mmHg at 25°C
Boiling Point:389.4°C at 760 mmHg
Flash Point:189.3°C
PSA：70.42000
Density:1.397g/cm³
LogP:2.79180

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5,6-Dihydro-6-oxophenanthridine-3-carboxylic acid

There total 6 articles about 5,6-Dihydro-6-oxophenanthridine-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 610-97-9
o-iodo-methyl-benzoic acid

: 39161-52-9
5[H]phenanthridin-6-one carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Cu / 8 h / 200 °C

2: NH₂NH₂; Raney nickel / methanol

3: 1 N aq. NaOH

With sodium hydroxide; nickel; copper; hydrazine; In methanol; 1: Ullmann coupling;
DOI:10.1016/S0960-894X(01)00281-5

Reference yield:

: 89976-27-2
methyl ester of 4-iodo-3-nitrobenzoic acid

: 39161-52-9
5[H]phenanthridin-6-one carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Cu / 8 h / 200 °C

2: NH₂NH₂; Raney nickel / methanol

3: 1 N aq. NaOH

With sodium hydroxide; nickel; copper; hydrazine; In methanol; 1: Ullmann coupling;
DOI:10.1016/S0960-894X(01)00281-5

Reference yield:

: 361444-27-1
2'-nitro-biphenyl-2,4'-dicarboxylic acid dimethyl ester

: 39161-52-9
5[H]phenanthridin-6-one carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: NH₂NH₂; Raney nickel / methanol

2: 1 N aq. NaOH

With sodium hydroxide; nickel; hydrazine; In methanol;
DOI:10.1016/S0960-894X(01)00281-5