1,1,3,3-Tetrabutyl-1,3-diphenoxydistannoxane

Base Information

• Chemical Name: 1,1,3,3-Tetrabutyl-1,3-diphenoxydistannoxane
• CAS No.: 27440-74-0
• Molecular Formula: C₂₈H₄₆O₃Sn₂
• Molecular Weight: 668.091
• DSSTox Substance ID: DTXSID50586884
• Wikidata: Q82479107

Synonyms:1,1,3,3-Tetrabutyl-1,3-diphenoxydistannoxane;27440-74-0;SCHEMBL465078;DTXSID50586884;1,3-diphenoxytetra-butyl distannoxane

Chemical Property of 1,1,3,3-Tetrabutyl-1,3-diphenoxydistannoxane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 18
• Exact Mass: 668.14850
• Heavy Atom Count: 33
• Complexity: 418

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC[Sn](CCCC)(OC1=CC=CC=C1)O[Sn](CCCC)(CCCC)OC2=CC=CC=C2

Technology Process of 1,1,3,3-Tetrabutyl-1,3-diphenoxydistannoxane

There total 1 articles about 1,1,3,3-Tetrabutyl-1,3-diphenoxydistannoxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1,1,3,3-tetrabutyl-1,3-di(phenoxy)distannoxane (27440-74-0)

Guidance literature:

Erhitzen v. Dibutyl-zinnoxid m. Phenol in Toluol;

DOI:10.1139/v63-174

Reference yield: 97.0%

{(C4H9)2Sn(O2CCF3)}2O (41311-29-9) + 1,1,3,3-tetrabutyl-1,3-di(phenoxy)distannoxane (27440-74-0) → (CF3CO2)(C4H9)2SnOSn(C4H9)2(OC6H5) (120477-31-8)

Guidance literature:

In hexane; molar ratio 1:1, gentle heating until homogeneous soln., then 15 h at -40°C; elem. anal.;

Reference yield: 79.0%

1,3-diacetoxy-1,1,3,3-tetrabutyldistannoxane (5967-09-9) + 1,1,3,3-tetrabutyl-1,3-di(phenoxy)distannoxane (27440-74-0) → (CH3CO2)(C4H9)2SnOSn(C4H9)2(OC6H5) (34072-44-1)

Guidance literature:

In hexane; gradually heating until homogeneous soln., cooling (-40°C), crystn. after 15 h; elem. anal.;

Downstream raw materials:

(CF₃CO₂)(C₄H₉)2SnOSn(C₄H₉)2(OC₆H₅)

(CH₃CO₂)(C₄H₉)2SnOSn(C₄H₉)2(OC₆H₅)

Tetra(n-butyl)-1-phenoxy-3-chlorodistannoxan

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