bis[N,N'-(2-chlorobenzylidene)ethylenediamine-κ2N,N']copper(I) dichlorocuprate(I) acetonitrile solvate

Base Information

• Chemical Name: bis[N,N'-(2-chlorobenzylidene)ethylenediamine-κ2N,N']copper(I) dichlorocuprate(I) acetonitrile solvate
• CAS No.: 1159215-82-3
• Molecular Formula: C₂H₃N*C₃₂H₂₈Cl₄CuN₄*Cl₂Cu
• Molecular Weight: 849.464
• Mol file: 1159215-82-3.mol

Synonyms:

Chemical Property of bis[N,N'-(2-chlorobenzylidene)ethylenediamine-κ2N,N']copper(I) dichlorocuprate(I) acetonitrile solvate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis[N,N'-(2-chlorobenzylidene)ethylenediamine-κ2N,N']copper(I) dichlorocuprate(I) acetonitrile solvate

There total 1 articles about bis[N,N'-(2-chlorobenzylidene)ethylenediamine-κ2N,N']copper(I) dichlorocuprate(I) acetonitrile solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-bis-(2-chloro-1-ylmethylenebenzene)-1,2-ethanediamine (348630-60-4) + acetonitrile (75-05-8,26809-02-9) + copper(l) chloride → bis[N,N'-(2-chlorobenzylidene)ethylenediamine-κ2N,N']copper(I) dichlorocuprate(I) acetonitrile solvate (1159215-82-3)

Guidance literature:

In acetonitrile; CuCl and diamine deriv. in CH3CN (molar ratio = 1:1) at room temp.; soln. concd. under vac., vapor diffusion of Et2O into soln.;

DOI:10.1107/S0108270107054960

upstream raw materials:

N,N'-bis-(2-chloro-1-ylmethylenebenzene)-1,2-ethanediamine

acetonitrile