3-Amino-6-chloro-2-hydroxy-benzenesulfonamide

Base Information

• Chemical Name: 3-Amino-6-chloro-2-hydroxy-benzenesulfonamide
• CAS No.: 276702-20-6
• Molecular Formula: C6H7ClN2O3S
• Molecular Weight: 222.652
• DSSTox Substance ID: DTXSID70463744
• Wikidata: Q82288766
• Mol file: 276702-20-6.mol

Synonyms:276702-20-6;3-amino-6-chloro-2-hydroxy-benzenesulfonamide;3-amino-6-chloro-2-hydroxybenzenesulfonamide;Benzenesulfonamide, 3-amino-6-chloro-2-hydroxy-;SCHEMBL4604015;DTXSID70463744;UALHUJCTSBPMRB-UHFFFAOYSA-N;3-amino-6-chloro-2hydroxybenzenesulfonamide;2-hydroxy-3-amino-6-chlorobenzenesulfonamide;FT-0737860;2-hydroxy-3-amino-6-chlorobenzene sulfonamide;A849735

Chemical Property of 3-Amino-6-chloro-2-hydroxy-benzenesulfonamide

Chemical Property:

• PSA: 114.79000
• LogP: 2.63750
• XLogP3: 0.6
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 1
• Exact Mass: 221.9865910
• Heavy Atom Count: 13
• Complexity: 276

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C(=C1N)O)S(=O)(=O)N)Cl

Technology Process of 3-Amino-6-chloro-2-hydroxy-benzenesulfonamide

There total 4 articles about 3-Amino-6-chloro-2-hydroxy-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-hydroxy-3-nitro-6-chlorobenzenesulfonamide (276702-19-3) + argon → 3-amino-6-chloro-2-hydroxybenzenesulfonamide (276702-20-6)

Guidance literature:

palladium-carbon; In ethyl acetate;

Reference yield: 91.0%

2-hydroxy-3-nitro-6-chlorobenzenesulfonamide (276702-19-3) → 3-amino-6-chloro-2-hydroxybenzenesulfonamide (276702-20-6)

Guidance literature:

With hydrogen; palladium-carbon; In ethyl acetate;

Reference yield: 75.0%

2-tert-butyl-6-chloro-benzooxazole-7-sulfonic acid amide (761448-08-2) → 3-amino-6-chloro-2-hydroxybenzenesulfonamide (276702-20-6)

Guidance literature:

With sulfuric acid; Heating;

DOI:10.1016/j.bmcl.2004.06.097

upstream raw materials:

2-tert-butyl-6-chloro-benzooxazole-7-sulfonic acid amide

2-hydroxy-3-nitro-6-chlorobenzenesulfonamide

Downstream raw materials:

N-(3-aminosulfonyl-4-chloro-2-hydroxyphenyl)-N'-phenethylurea

N-(3-aminosulfonyl-4-chloro-2-hydroxyphenyl)-N'-(3,5-dimethylisoxazol4-yl)urea

N-(3-aminosulfonyl4-chloro-2-hydroxyphenyl)-N'-(2-methyl)benzylurea

6-Chloro-2-hydroxy-3-(3-piperidin-4-yl-ureido)-benzenesulfonamide

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