PhCH₂-thiolatopentachlorotungsten(VI)

Base Information

• Chemical Name: PhCH₂-thiolatopentachlorotungsten(VI)
• CAS No.: 73432-37-8
• Molecular Formula: C₇H₇Cl₅SW
• Molecular Weight: 484.314
• Mol file: 73432-37-8.mol

Synonyms:

Chemical Property of PhCH₂-thiolatopentachlorotungsten(VI)

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of PhCH₂-thiolatopentachlorotungsten(VI)

There total 1 articles about PhCH₂-thiolatopentachlorotungsten(VI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzylthiotrimethylsilane (14629-67-5) + tungsten(VI) chloride (13283-01-7) → WSCl4 (25127-53-1) + PhCH2-thiolatopentachlorotungsten(VI) (73432-37-8)

Guidance literature:

In carbon disulfide; byproducts: Me3SiCl, (PhCH2S)2, Me3CCl; stoich. amt. of silyl reagent soln. added to WCl6 soln. under inert atm. , then stirred for 15-20 min (by decomposition study for 12 h), volumereduced until pptn.; filtered, washed with hexane, dried in vac., elem. anal.;

DOI:10.1039/DT9800000257

upstream raw materials:

benzylthiotrimethylsilane

tungsten(VI) chloride