Methanone, (3,5-diphenyl-2-thienyl)phenyl-

Base Information

• Chemical Name: Methanone, (3,5-diphenyl-2-thienyl)phenyl-
• CAS No.: 27895-87-0
• Molecular Formula: C23H16OS
• Molecular Weight: 340.445
• DSSTox Substance ID: DTXSID20481731
• Nikkaji Number: J1.934.523H
• Wikidata: Q82317323
• Mol file: 27895-87-0.mol

Synonyms:Methanone, (3,5-diphenyl-2-thienyl)phenyl-;27895-87-0;2-benzoyl-3,5-diphenylthiophene;DTXSID20481731

Chemical Property of Methanone, (3,5-diphenyl-2-thienyl)phenyl-

Chemical Property:

• XLogP3: 6.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 340.09218630
• Heavy Atom Count: 25
• Complexity: 429

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=CC(=C(S2)C(=O)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of Methanone, (3,5-diphenyl-2-thienyl)phenyl-

There total 8 articles about Methanone, (3,5-diphenyl-2-thienyl)phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2,4,6-triphenylpyrylium tetrafluoroborate (448-61-3) → 2-benzoyl-3,5-diphenylthiophene (27895-87-0)

Guidance literature:

2,4,6-triphenylpyrylium tetrafluoroborate; With sodium sulfide; In water; acetone; at 20 ℃; for 0.0833333h;

With iodine; In water; acetone; at 20 ℃; for 0.0333333h;

DOI:10.1081/SCC-120022174

Reference yield: 65.0%

2,4,6-triphenyl-4H-thiopyran (7584-36-3) → 2-benzoyl-3,5-diphenylthiophene (27895-87-0)

Guidance literature:

With pyridine; selenium(IV) oxide; 1) 2h, reflux, 2) 3h, reflux;

DOI:10.1007/BF00470019

Reference yield: 62.0%

bromobenzene (108-86-1,52753-63-6) + 2-Benzoylthiophene (135-00-2) → 2-benzoyl-3,5-diphenylthiophene (27895-87-0) + phenyl (5-phenylthiophen-2-yl) methanone (13858-68-9)

Guidance literature:

With palladium diacetate; P(O-biphenyl)(t-Bu)2; caesium carbonate; In o-xylene; for 65h; Heating;

DOI:10.1021/ja0259279

upstream raw materials:

2,4,6-triphenyl-4H-thiopyran

2,4,6-Triphenylthiapyrylium trifluoroacetate

bromobenzene

2-Benzoylthiophene

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