4-[Bis(2-methoxyethyl)amino]benzaldehyde

Base Information

Chemical Name:4-[Bis(2-methoxyethyl)amino]benzaldehyde
CAS No.:27913-87-7
Molecular Formula:C13H19NO3
Molecular Weight:237.299
Hs Code.:
DSSTox Substance ID:DTXSID60708752
Nikkaji Number:J2.898.068J
Wikidata:Q82643282
Mol file:27913-87-7.mol

Synonyms:4-[Bis(2-methoxyethyl)amino]benzaldehyde;27913-87-7;Benzaldehyde, 4-[bis(2-methoxyethyl)amino]-;SCHEMBL1444357;DTXSID60708752;AKOS010678919;4-[bis-(2-methoxyethyl)amino]benzaldehyde

Suppliers and Price of 4-[Bis(2-methoxyethyl)amino]benzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[Bis(2-methoxyethyl)amino]benzaldehyde

Chemical Property:

PSA：38.77000
LogP:1.59830
XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:237.13649347
Heavy Atom Count:17
Complexity:195

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COCCN(CCOC)C1=CC=C(C=C1)C=O

Technology Process of 4-[Bis(2-methoxyethyl)amino]benzaldehyde

There total 3 articles about 4-[Bis(2-methoxyethyl)amino]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 87182-67-0
N,N-bis(2-methoxyethyl)-benzenamide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 27913-87-7
4-(bis-(2-methoxyethyl)amino)benzaldehyde

Guidance literature:: With trichlorophosphate; at 0 - 20 ℃; Inert atmosphere;

Reference yield: 5.0%

: 111-95-5
Bis-(2-methoxyethyl)amine

: 459-57-4
4-fluorobenzaldehyde

: 27913-87-7
4-(bis-(2-methoxyethyl)amino)benzaldehyde

Guidance literature:: With caesium carbonate; In dimethyl sulfoxide; at 160 ℃; for 1h; Microwave irradiation;
DOI:10.2478/s11696-012-0251-2

Reference yield:

: 62-53-3
aniline

: 27913-87-7
4-(bis-(2-methoxyethyl)amino)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; potassium iodide / N,N-dimethyl-formamide / 100 °C / Inert atmosphere

2: trichlorophosphate / 0 - 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; potassium iodide; trichlorophosphate; In N,N-dimethyl-formamide;